N-(4-ethoxyphenyl)-2-nitrobenzamide

Base Information

• Chemical Name: N-(4-ethoxyphenyl)-2-nitrobenzamide
• CAS No.: 316142-72-0
• Molecular Formula: C₁₅H₁₄N₂O₄
• Molecular Weight: 286.287
• Mol file: 316142-72-0.mol

Synonyms:2-nitro-benzoic acid p-phenetidide

Chemical Property of N-(4-ethoxyphenyl)-2-nitrobenzamide

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

N-(4-Ethoxyphenyl)-2-nitrobenzamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(4-ethoxyphenyl)-2-nitrobenzamide

There total 1 articles about N-(4-ethoxyphenyl)-2-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Ethoxyaniline (156-43-4) + 2-nitrobenzyl chloride (610-14-0) → 2-nitro-benzoic acid p-phenetidide (316142-72-0)

Guidance literature:

With pyridine;

Reference yield: 94.0%

carbon monoxide (201230-82-2) + 2-nitro-benzoic acid p-phenetidide (316142-72-0) → 3-(4-ethoxy-phenyl)-1H-quinazoline-2,4-dione (2400-98-8)

Guidance literature:

With selenium; triethylamine; In tetrahydrofuran; at 170 ℃; for 11h; under 15001.5 Torr;

DOI:10.1016/j.tetlet.2010.01.040

Reference yield:

2-nitro-benzoic acid p-phenetidide (316142-72-0) → 2-nitro-benzoic acid-(4-ethoxy-2-nitro-anilide) + 2-nitro-benzoic acid-(4-ethoxy-3-nitro-anilide)

Guidance literature:

With nitric acid; acetic acid;

upstream raw materials:

4-Ethoxyaniline

2-nitrobenzyl chloride

Downstream raw materials:

3-(4-ethoxy-phenyl)-1H-quinazoline-2,4-dione

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