4-benzyloxy-2-benzoyloxymethyl-2-hydroxybutyl benzoate

Base Information

Chemical Name:4-benzyloxy-2-benzoyloxymethyl-2-hydroxybutyl benzoate
CAS No.:119117-27-0
Molecular Formula:C₂₆H₂₆O₆
Molecular Weight:434.489
Hs Code.:

Synonyms:4-benzyloxy-2-benzoyloxymethyl-2-hydroxybutyl benzoate

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Chemical Property of 4-benzyloxy-2-benzoyloxymethyl-2-hydroxybutyl benzoate

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Technology Process of 4-benzyloxy-2-benzoyloxymethyl-2-hydroxybutyl benzoate

There total 3 articles about 4-benzyloxy-2-benzoyloxymethyl-2-hydroxybutyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 98-88-4
benzoyl chloride

: 119117-21-4
4-benzyloxy-2-hydroxymethylbutane-1,2-diol

: 119117-28-1
4-benzyloxy-2-hydroxy-2-hydroxymethylbutyl benzoate

: 119117-27-0
4-benzyloxy-2-benzoyloxymethyl-2-hydroxybutyl benzoate

Guidance literature:: With pyridine; at 25 ℃; for 2h;

Reference yield:

: 1462-37-9
bromoethyl-2-benzyl ether

: 119117-27-0
4-benzyloxy-2-benzoyloxymethyl-2-hydroxybutyl benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium hydride / 1.) DMF, 25 deg C, 1 h; 2.) DMF, 25 deg C, 16 h

2: 88 percent / lithium aluminium hydride / tetrahydrofuran / 2 h / 25 °C

3: 67 percent / pyridine / 2 h / 25 °C

With pyridine; lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran;

Reference yield:

: 119117-20-3
diethyl acetoxy(2-benzyloxyethyl)malonate

: 119117-27-0
4-benzyloxy-2-benzoyloxymethyl-2-hydroxybutyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / lithium aluminium hydride / tetrahydrofuran / 2 h / 25 °C

2: 67 percent / pyridine / 2 h / 25 °C

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran;