N'-[4-(2-{2-[4-(2-cyano-ethylamino)furazan-3-yl]benzoimidazol-1-yl}acetyl)phenyl]-N,N-dimethyl-formamidine

Base Information

Chemical Name:N'-[4-(2-{2-[4-(2-cyano-ethylamino)furazan-3-yl]benzoimidazol-1-yl}acetyl)phenyl]-N,N-dimethyl-formamidine
CAS No.:1263384-40-2
Molecular Formula:C₂₃H₂₂N₈O₂
Molecular Weight:442.48
Hs Code.:

Synonyms:N'-[4-(2-{2-[4-(2-cyano-ethylamino)furazan-3-yl]benzoimidazol-1-yl}acetyl)phenyl]-N,N-dimethyl-formamidine

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Chemical Property of N'-[4-(2-{2-[4-(2-cyano-ethylamino)furazan-3-yl]benzoimidazol-1-yl}acetyl)phenyl]-N,N-dimethyl-formamidine

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Technology Process of N'-[4-(2-{2-[4-(2-cyano-ethylamino)furazan-3-yl]benzoimidazol-1-yl}acetyl)phenyl]-N,N-dimethyl-formamidine

There total 9 articles about N'-[4-(2-{2-[4-(2-cyano-ethylamino)furazan-3-yl]benzoimidazol-1-yl}acetyl)phenyl]-N,N-dimethyl-formamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 332026-86-5
3-amino-4-(1H-benzo[d]imidazol-2-yl)-1,2,5-oxadiazole

: 1263384-40-2
N'-[4-(2-{2-[4-(2-cyano-ethylamino)furazan-3-yl]benzoimidazol-1-yl}acetyl)phenyl]-N,N-dimethyl-formamidine

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium methylate / pyridine; methanol / 20 °C / Cooling with ice

2.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 20 °C

3.1: hydrogen / palladium 10% on activated carbon / ethyl acetate; methanol / 3 h / 20 °C / 760.05 Torr

4.1: N-ethyl-N,N-diisopropylamine; trichlorophosphate / -10 - 20 °C

4.2: 0 - 20 °C / pH 11

With hydrogen; sodium methylate; potassium carbonate; N-ethyl-N,N-diisopropylamine; trichlorophosphate; palladium 10% on activated carbon; In pyridine; methanol; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 798577-91-0
3-(4-{1-[2-(4-amino-phenyl)-2-oxo-ethyl]-1H-benzoimidazol-2-yl}-furazan-3-ylamino)-propionitrile

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1263384-40-2
N'-[4-(2-{2-[4-(2-cyano-ethylamino)furazan-3-yl]benzoimidazol-1-yl}acetyl)phenyl]-N,N-dimethyl-formamidine

Guidance literature:: 3-(4-{1-[2-(4-amino-phenyl)-2-oxo-ethyl]-1H-benzoimidazol-2-yl}-furazan-3-ylamino)-propionitrile; N,N-dimethyl-formamide; With N-ethyl-N,N-diisopropylamine; trichlorophosphate; at -10 - 20 ℃;

With sodium hydroxide; In water; acetonitrile; at 0 - 20 ℃; pH=11;

Reference yield:

: 72531-10-3
4-<<(benzyloxy)carbonyl>amino>acetophenone

: 1263384-40-2
N'-[4-(2-{2-[4-(2-cyano-ethylamino)furazan-3-yl]benzoimidazol-1-yl}acetyl)phenyl]-N,N-dimethyl-formamidine

Guidance literature:: Multi-step reaction with 4 steps

1.1: copper(ll) bromide / ethanol / 2 h / Reflux

2.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 20 °C

3.1: hydrogen / palladium 10% on activated carbon / ethyl acetate; methanol / 3 h / 20 °C / 760.05 Torr

4.1: N-ethyl-N,N-diisopropylamine; trichlorophosphate / -10 - 20 °C

4.2: 0 - 20 °C / pH 11

With hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine; copper(ll) bromide; trichlorophosphate; palladium 10% on activated carbon; In methanol; ethanol; ethyl acetate; N,N-dimethyl-formamide;