benzyl 2-(5-(2-chloropyridin-4-yl)-2-methyl-3-(2-(phenylsulfonyl)benzyl)-1H-pyrrol-1-yl)acetate

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Chemical Name:benzyl 2-(5-(2-chloropyridin-4-yl)-2-methyl-3-(2-(phenylsulfonyl)benzyl)-1H-pyrrol-1-yl)acetate
CAS No.:1312717-82-0
Molecular Formula:C₃₂H₂₇ClN₂O₄S
Molecular Weight:571.096
Hs Code.:

Synonyms:benzyl 2-(5-(2-chloropyridin-4-yl)-2-methyl-3-(2-(phenylsulfonyl)benzyl)-1H-pyrrol-1-yl)acetate

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Chemical Property of benzyl 2-(5-(2-chloropyridin-4-yl)-2-methyl-3-(2-(phenylsulfonyl)benzyl)-1H-pyrrol-1-yl)acetate

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Technology Process of benzyl 2-(5-(2-chloropyridin-4-yl)-2-methyl-3-(2-(phenylsulfonyl)benzyl)-1H-pyrrol-1-yl)acetate

There total 3 articles about benzyl 2-(5-(2-chloropyridin-4-yl)-2-methyl-3-(2-(phenylsulfonyl)benzyl)-1H-pyrrol-1-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1312717-81-9
benzyl 2-(2-(2-chloropyridin-4-yl)-5-methyl-1H-pyrrol-1-yl)acetate

: 126076-76-4
2-(phenylsulfonyl)benzaldehyde

: 1312717-82-0
benzyl 2-(5-(2-chloropyridin-4-yl)-2-methyl-3-(2-(phenylsulfonyl)benzyl)-1H-pyrrol-1-yl)acetate

Guidance literature:: benzyl 2-(2-(2-chloropyridin-4-yl)-5-methyl-1H-pyrrol-1-yl)acetate; With triethylsilane; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 ℃; for 0.166667h;

2-(phenylsulfonyl)benzaldehyde; In dichloromethane; at -78 - 20 ℃;

Reference yield:

: 101066-61-9
2-chloropyridine-4-carbaldehyde

: 1312717-82-0
benzyl 2-(5-(2-chloropyridin-4-yl)-2-methyl-3-(2-(phenylsulfonyl)benzyl)-1H-pyrrol-1-yl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide / ethanol / 18.5 h / 85 °C

2.1: sodium hydrogencarbonate / dichloromethane / 278 h / 45 - 65 °C

3.1: trimethylsilyl trifluoromethanesulfonate; triethylsilane / dichloromethane / 0.17 h / -78 °C

3.2: -78 - 20 °C

With triethylsilane; trimethylsilyl trifluoromethanesulfonate; sodium hydrogencarbonate; 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; triethylamine; In ethanol; dichloromethane;

Reference yield:

: 898785-30-3
1-(2-chloropyridin-4-yl)pentane-1,4-dione

: 1312717-82-0
benzyl 2-(5-(2-chloropyridin-4-yl)-2-methyl-3-(2-(phenylsulfonyl)benzyl)-1H-pyrrol-1-yl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydrogencarbonate / dichloromethane / 278 h / 45 - 65 °C

2.1: trimethylsilyl trifluoromethanesulfonate; triethylsilane / dichloromethane / 0.17 h / -78 °C

2.2: -78 - 20 °C

With triethylsilane; trimethylsilyl trifluoromethanesulfonate; sodium hydrogencarbonate; In dichloromethane;