C₁₃H₁₇NO

Base Information

• Chemical Name: C₁₃H₁₇NO
• CAS No.: 742673-63-8
• Molecular Formula: C₁₃H₁₇NO
• Molecular Weight: 203.284
• Mol file: 742673-63-8.mol

Synonyms:C₁₃H₁₇NO

Chemical Property of C₁₃H₁₇NO

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₁₃H₁₇NO

There total 2 articles about C₁₃H₁₇NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzamide (55-21-0,27208-38-4) + hexanal (66-25-1) → 2-butyl-oct-2-en-1-al (64935-38-2,99915-14-7,13019-16-4) + N-(hex-1en-1-yl)benzamide + N-hexylbenzamide (4773-75-5) + C13H17NO (742673-63-8) + C20H24N2O2 (157944-94-0) + C19H29NO + C26H34N2O2 + hexan-1-ol (111-27-3)

Guidance literature:

With chloro(1,5-cyclooctadiene)rhodium(I) dimer; hydrogen; toluene-4-sulfonic acid; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In diethylene glycol dimethyl ether; at 80 ℃; for 10h; under 60006 Torr; Time; Autoclave; Schlenk technique; Inert atmosphere;

DOI:10.1002/adsc.201200837

Reference yield:

1-penten (109-67-1) + carbon monoxide (201230-82-2) + benzamide (55-21-0,27208-38-4) → heptanal (111-71-7) + N-(hex-1en-1-yl)benzamide + N-hexylbenzamide (4773-75-5) + C13H17NO (742673-63-8) + C13H17NO + C13H17NO

Guidance literature:

With dicarbonylacetylacetonato rhodium (I); hydrogen; toluene-4-sulfonic acid; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In diethylene glycol dimethyl ether; at 100 ℃; for 8h; under 37503.8 Torr; chemoselective reaction; Inert atmosphere; Schlenk technique;

DOI:10.1002/cssc.201300484

Reference yield:

C13H17NO (742673-63-8) + tris-iso-propylsilyl acetylene (89343-06-6) → C24H39NOSi + C24H39NOSi

Guidance literature:

With bis(1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate; (R)-(6,6'-dimethoxy-[1,1'-biphenyl]-2,2'-diyl)bis(diisopropylphosphine); In tetrahydrofuran; at 60 ℃; for 12h; Overall yield = 12 %; enantioselective reaction; Inert atmosphere; Sealed tube;

DOI:10.1021/jacs.7b12054

upstream raw materials:

benzamide

hexanal

1-penten

carbon monoxide