Imidazole-1-carbothioic acid O-[(1R,2R,6S)-6-(3-phenyl-propyl)-7-oxa-bicyclo[4.1.0]hept-2-yl] ester

Base Information

• Chemical Name: Imidazole-1-carbothioic acid O-[(1R,2R,6S)-6-(3-phenyl-propyl)-7-oxa-bicyclo[4.1.0]hept-2-yl] ester
• CAS No.: 129152-09-6
• Molecular Formula: C₁₉H₂₂N₂O₂S
• Molecular Weight: 342.462

Synonyms:Imidazole-1-carbothioic acid O-[(1R,2R,6S)-6-(3-phenyl-propyl)-7-oxa-bicyclo[4.1.0]hept-2-yl] ester

Chemical Property of Imidazole-1-carbothioic acid O-[(1R,2R,6S)-6-(3-phenyl-propyl)-7-oxa-bicyclo[4.1.0]hept-2-yl] ester

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Technology Process of Imidazole-1-carbothioic acid O-[(1R,2R,6S)-6-(3-phenyl-propyl)-7-oxa-bicyclo[4.1.0]hept-2-yl] ester

There total 4 articles about Imidazole-1-carbothioic acid O-[(1R,2R,6S)-6-(3-phenyl-propyl)-7-oxa-bicyclo[4.1.0]hept-2-yl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-Ethoxycyclohex-2-en-1-one (5323-87-5) → Imidazole-1-carbothioic acid O-[(1R,2R,6S)-6-(3-phenyl-propyl)-7-oxa-bicyclo[4.1.0]hept-2-yl] ester (129152-09-6)

Guidance literature:

Multi-step reaction with 4 steps

1: 1) Mg / 1) THF

2: NaBH₄, CeCl₃*7H₂O / methanol

3: MCPBA / CH₂Cl₂ / Ambient temperature

4: DMAP / CH₂Cl₂

With dmap; sodium tetrahydroborate; cerium(III) chloride; magnesium; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane;

DOI:10.1021/jo00305a001

Reference yield:

3-(3-Phenyl-propyl)-cyclohex-2-enol → Imidazole-1-carbothioic acid O-[(1R,2R,6S)-6-(3-phenyl-propyl)-7-oxa-bicyclo[4.1.0]hept-2-yl] ester (129152-09-6)

Guidance literature:

Multi-step reaction with 2 steps

1: MCPBA / CH₂Cl₂ / Ambient temperature

2: DMAP / CH₂Cl₂

With dmap; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

DOI:10.1021/jo00305a001

Reference yield:

3-(3-Phenyl-propyl)-cyclohex-2-enone (144730-06-3) → Imidazole-1-carbothioic acid O-[(1R,2R,6S)-6-(3-phenyl-propyl)-7-oxa-bicyclo[4.1.0]hept-2-yl] ester (129152-09-6)

Guidance literature:

Multi-step reaction with 3 steps

1: NaBH₄, CeCl₃*7H₂O / methanol

2: MCPBA / CH₂Cl₂ / Ambient temperature

3: DMAP / CH₂Cl₂

With dmap; sodium tetrahydroborate; cerium(III) chloride; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane;

DOI:10.1021/jo00305a001

upstream raw materials:

1,1'-Thiocarbonyldiimidazole

3-Ethoxycyclohex-2-en-1-one

3-(3-Phenyl-propyl)-cyclohex-2-enone

Downstream raw materials:

(3aR,7aR)-1-Phenyl-octahydro-inden-3a-ol

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