(R)-(-)-2,4-bis-ethoxymethoxy-6-methylbenzoic acid 1-methylbut-3-enyl ester

Base Information

Chemical Name:(R)-(-)-2,4-bis-ethoxymethoxy-6-methylbenzoic acid 1-methylbut-3-enyl ester
CAS No.:853645-36-0
Molecular Formula:C₁₉H₂₈O₆
Molecular Weight:352.428
Hs Code.:

Synonyms:(R)-(-)-2,4-bis-ethoxymethoxy-6-methylbenzoic acid 1-methylbut-3-enyl ester

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Chemical Property of (R)-(-)-2,4-bis-ethoxymethoxy-6-methylbenzoic acid 1-methylbut-3-enyl ester

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Technology Process of (R)-(-)-2,4-bis-ethoxymethoxy-6-methylbenzoic acid 1-methylbut-3-enyl ester

There total 3 articles about (R)-(-)-2,4-bis-ethoxymethoxy-6-methylbenzoic acid 1-methylbut-3-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 480-64-8
orsellinic acid

: 853645-36-0
(R)-(-)-2,4-bis-ethoxymethoxy-6-methylbenzoic acid 1-methylbut-3-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: tris(3-chlorophenyl)phosphine; ethoxycarbonylazocarboxymethyl polystyrene / CH₂Cl₂ / 0.5 h / 23 °C

2: diisopropylethylamine / tetrabutylammonium iodide / dimethylformamide / 5 h / 80 °C

With ethoxycarbonylazocarboxymethyl polystyrene; tri(m-chlorophenyl)-phosphine; N-ethyl-N,N-diisopropylamine; tetra-(n-butyl)ammonium iodide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.200600553

Reference yield:

: 625-31-0,64584-92-5,111957-98-3,55563-79-6
(S)-4-penten-2-ol

: 853645-36-0
(R)-(-)-2,4-bis-ethoxymethoxy-6-methylbenzoic acid 1-methylbut-3-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / tris(3-chlorophenyl)phosphine; PS-DEAD / toluene / 0.17 h / 20 °C

2: 95 percent / tetrabutylammonium iodide; iPr₂NEt / dimethylformamide / 80 °C

With PS-DEAD; tri(m-chlorophenyl)-phosphine; tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; toluene; 1: Mitsunobu reaction;
DOI:10.1021/ja043101w

Reference yield:

: 64584-92-5
(R)-pent-4-en-2-ol

: 853645-36-0
(R)-(-)-2,4-bis-ethoxymethoxy-6-methylbenzoic acid 1-methylbut-3-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: tris(3-chlorophenyl)phosphine; ethoxycarbonylazocarboxymethyl polystyrene / CH₂Cl₂ / 0.5 h / 23 °C

2: diisopropylethylamine / tetrabutylammonium iodide / dimethylformamide / 5 h / 80 °C

With ethoxycarbonylazocarboxymethyl polystyrene; tri(m-chlorophenyl)-phosphine; N-ethyl-N,N-diisopropylamine; tetra-(n-butyl)ammonium iodide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.200600553