4-Allyl-1-benzyl-2-methyl-7-oxo-4,7-dihydro-1H-pyrrolo[3,2-b]pyridine-3,6-dicarboxylic acid 3-methyl ester

Base Information

Chemical Name:4-Allyl-1-benzyl-2-methyl-7-oxo-4,7-dihydro-1H-pyrrolo[3,2-b]pyridine-3,6-dicarboxylic acid 3-methyl ester
CAS No.:97653-49-1
Molecular Formula:C₂₁H₂₀N₂O₅
Molecular Weight:380.4
Hs Code.:

Synonyms:4-Allyl-1-benzyl-2-methyl-7-oxo-4,7-dihydro-1H-pyrrolo[3,2-b]pyridine-3,6-dicarboxylic acid 3-methyl ester

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Chemical Property of 4-Allyl-1-benzyl-2-methyl-7-oxo-4,7-dihydro-1H-pyrrolo[3,2-b]pyridine-3,6-dicarboxylic acid 3-methyl ester

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Technology Process of 4-Allyl-1-benzyl-2-methyl-7-oxo-4,7-dihydro-1H-pyrrolo[3,2-b]pyridine-3,6-dicarboxylic acid 3-methyl ester

There total 5 articles about 4-Allyl-1-benzyl-2-methyl-7-oxo-4,7-dihydro-1H-pyrrolo[3,2-b]pyridine-3,6-dicarboxylic acid 3-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 97653-37-7
4-Allyl-1-benzyl-2-methyl-7-oxo-4,7-dihydro-1H-pyrrolo[3,2-b]pyridine-3,6-dicarboxylic acid 6-ethyl ester 3-methyl ester

: 97653-49-1
4-Allyl-1-benzyl-2-methyl-7-oxo-4,7-dihydro-1H-pyrrolo[3,2-b]pyridine-3,6-dicarboxylic acid 3-methyl ester

Guidance literature:: With sodium hydroxide; In methanol; for 1h; heated on a boiling water bath;
DOI:10.1002/jhet.5570220122

Reference yield:

: 100-39-0
benzyl bromide

: 97653-49-1
4-Allyl-1-benzyl-2-methyl-7-oxo-4,7-dihydro-1H-pyrrolo[3,2-b]pyridine-3,6-dicarboxylic acid 3-methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / sodium methoxide / dimethylformamide / 1 h / Ambient temperature

2: 87 percent / Dowtherm A / 0.5 h / Heating

3: 95.5 percent / sodium methoxide / dimethylformamide / Ambient temperature; overnight

4: 80 percent / 1percent aq. sodium hydroxide / methanol / 1 h / heated on a boiling water bath

With sodium hydroxide; diphenyl ether-biphenyl eutectic; sodium methylate; In methanol; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570220122

Reference yield:

: 97653-29-7
N-<2-Methyl-3-carbomethoxypyrrol-4-yl>aminomethylenemalonic Acid, Diethyl Ester

: 97653-49-1
4-Allyl-1-benzyl-2-methyl-7-oxo-4,7-dihydro-1H-pyrrolo[3,2-b]pyridine-3,6-dicarboxylic acid 3-methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / sodium methoxide / dimethylformamide / 1 h / Ambient temperature

2: 87 percent / Dowtherm A / 0.5 h / Heating

3: 95.5 percent / sodium methoxide / dimethylformamide / Ambient temperature; overnight

4: 80 percent / 1percent aq. sodium hydroxide / methanol / 1 h / heated on a boiling water bath

With sodium hydroxide; diphenyl ether-biphenyl eutectic; sodium methylate; In methanol; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570220122