4-Allyl-1-benzyl-2-methyl-7-oxo-4,7-dihydro-1H-pyrrolo[3,2-b]pyridine-3,6-dicarboxylic acid 6-ethyl ester 3-methyl ester

Base Information

Chemical Name:4-Allyl-1-benzyl-2-methyl-7-oxo-4,7-dihydro-1H-pyrrolo[3,2-b]pyridine-3,6-dicarboxylic acid 6-ethyl ester 3-methyl ester
CAS No.:97653-37-7
Molecular Formula:C₂₃H₂₄N₂O₅
Molecular Weight:408.454
Hs Code.:

Synonyms:4-Allyl-1-benzyl-2-methyl-7-oxo-4,7-dihydro-1H-pyrrolo[3,2-b]pyridine-3,6-dicarboxylic acid 6-ethyl ester 3-methyl ester

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Chemical Property of 4-Allyl-1-benzyl-2-methyl-7-oxo-4,7-dihydro-1H-pyrrolo[3,2-b]pyridine-3,6-dicarboxylic acid 6-ethyl ester 3-methyl ester

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Technology Process of 4-Allyl-1-benzyl-2-methyl-7-oxo-4,7-dihydro-1H-pyrrolo[3,2-b]pyridine-3,6-dicarboxylic acid 6-ethyl ester 3-methyl ester

There total 5 articles about 4-Allyl-1-benzyl-2-methyl-7-oxo-4,7-dihydro-1H-pyrrolo[3,2-b]pyridine-3,6-dicarboxylic acid 6-ethyl ester 3-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.5%

: 97654-63-2
1-Benzyl-2-methyl-3-carbomethoxy-6-carbethoxy-7-hydroxypyrrolo<3,2-b>pyridine

: 106-95-6
allyl bromide

: 97653-37-7
4-Allyl-1-benzyl-2-methyl-7-oxo-4,7-dihydro-1H-pyrrolo[3,2-b]pyridine-3,6-dicarboxylic acid 6-ethyl ester 3-methyl ester

Guidance literature:: With sodium methylate; In N,N-dimethyl-formamide; Ambient temperature; overnight;
DOI:10.1002/jhet.5570220122

Reference yield:

: 100-39-0
benzyl bromide

: 97653-37-7
4-Allyl-1-benzyl-2-methyl-7-oxo-4,7-dihydro-1H-pyrrolo[3,2-b]pyridine-3,6-dicarboxylic acid 6-ethyl ester 3-methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / sodium methoxide / dimethylformamide / 1 h / Ambient temperature

2: 87 percent / Dowtherm A / 0.5 h / Heating

3: 95.5 percent / sodium methoxide / dimethylformamide / Ambient temperature; overnight

With diphenyl ether-biphenyl eutectic; sodium methylate; In N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570220122

Reference yield:

: 97653-29-7
N-<2-Methyl-3-carbomethoxypyrrol-4-yl>aminomethylenemalonic Acid, Diethyl Ester

: 97653-37-7
4-Allyl-1-benzyl-2-methyl-7-oxo-4,7-dihydro-1H-pyrrolo[3,2-b]pyridine-3,6-dicarboxylic acid 6-ethyl ester 3-methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / sodium methoxide / dimethylformamide / 1 h / Ambient temperature

2: 87 percent / Dowtherm A / 0.5 h / Heating

3: 95.5 percent / sodium methoxide / dimethylformamide / Ambient temperature; overnight

With diphenyl ether-biphenyl eutectic; sodium methylate; In N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570220122