Technology Process of C24H36FN3O2
There total 7 articles about C24H36FN3O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium(II) hydroxide/carbon; palladium 10% on activated carbon;
In
ethanol;
at 20 ℃;
for 21h;
under 760.051 Torr;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: copper(l) iodide / tetrahydrofuran / 3 h / 0 °C
2.1: sodium hydroxide / ethanol; water / 15 h / 20 °C
2.2: 0 °C / pH 3
3.1: copper(I) oxide / acetonitrile / 1 - 1.25 h / Heating / reflux
4.1: diisobutylaluminium hydride / dichloromethane / 4 h / -78 - -60 °C
5.1: sodium tris(acetoxy)borohydride / dichloromethane / 2 h / 20 °C
6.1: hydrogen / palladium 10% on activated carbon; palladium(II) hydroxide/carbon / ethanol / 21 h / 20 °C / 760.05 Torr
With
copper(I) oxide; sodium hydroxide; hydrogen; sodium tris(acetoxy)borohydride; diisobutylaluminium hydride;
copper(l) iodide; palladium(II) hydroxide/carbon; palladium 10% on activated carbon;
In
tetrahydrofuran; ethanol; dichloromethane; water; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium tris(acetoxy)borohydride / dichloromethane / 2 h / 20 °C
2: hydrogen / palladium 10% on activated carbon; palladium(II) hydroxide/carbon / ethanol / 21 h / 20 °C / 760.05 Torr
With
hydrogen; sodium tris(acetoxy)borohydride;
palladium(II) hydroxide/carbon; palladium 10% on activated carbon;
In
ethanol; dichloromethane;
