N-(2,6-dimethylphenyl)-2-methylbenzamide

Base Information

Chemical Name:N-(2,6-dimethylphenyl)-2-methylbenzamide
CAS No.:34743-34-5
Molecular Formula:C₁₆H₁₇NO
Molecular Weight:239.317
Hs Code.:
European Community (EC) Number:666-031-2
Mol file:34743-34-5.mol

Synonyms:N-(2,6-dimethylphenyl)-2-methylbenzamide;2,2',6'-TRIMETHYLBENZANILIDE;Cambridge id 7135579;STK209444;AKOS001293372;AN-652/41018791;Z27073206

Suppliers and Price of N-(2,6-dimethylphenyl)-2-methylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2,2',6'-TRIMETHYLBENZANILIDE 95.00%
5MG
$ 497.06

Total 0 raw suppliers

Chemical Property of N-(2,6-dimethylphenyl)-2-methylbenzamide

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:239.131014166
Heavy Atom Count:18
Complexity:279

Purity/Quality:: 2,2',6'-TRIMETHYLBENZANILIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(C(=CC=C1)C)NC(=O)C2=CC=CC=C2C

Technology Process of N-(2,6-dimethylphenyl)-2-methylbenzamide

There total 8 articles about N-(2,6-dimethylphenyl)-2-methylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 615-37-2
ortho-methylphenyl iodide

: 201230-82-2
carbon monoxide

: 87-62-7
2,6-dimethylaniline

: 34743-34-5
N-(2,6-dimethylphenyl)-2-methylbenzamide

Guidance literature:: With bis(tri-t-butylphosphine)palladium⁽⁰⁾; tetrabutyl-ammonium chloride; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; for 20h; under 1535.79 Torr; Schlenk technique; Inert atmosphere;
DOI:10.1021/ja4098093

Reference yield: 93.0%

: tert-butyl (2-methylbenzoyl)(phenyl)carbamate

: 87-62-7
2,6-dimethylaniline

: 34743-34-5
N-(2,6-dimethylphenyl)-2-methylbenzamide

Guidance literature:: With (3-phenylallyl)(chloro)-[1,3-bis(2,6-diisopropylphenyl)-4,5-dihydroimidazol-2-ylidene]palladium(II); potassium carbonate; In 1,2-dimethoxyethane; at 110 ℃; for 15h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.7b00796

Reference yield:

: 7055-03-0
2-methyl-N-phenylbenzamide

: 34743-34-5
N-(2,6-dimethylphenyl)-2-methylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: dmap / dichloromethane / 15 h / 20 °C / Inert atmosphere; Schlenk technique

2: potassium carbonate; (3-phenylallyl)(chloro)-[1,3-bis(2,6-diisopropylphenyl)-4,5-dihydroimidazol-2-ylidene]palladium(II) / 1,2-dimethoxyethane / 15 h / 110 °C / Schlenk technique; Inert atmosphere

With dmap; (3-phenylallyl)(chloro)-[1,3-bis(2,6-diisopropylphenyl)-4,5-dihydroimidazol-2-ylidene]palladium(II); potassium carbonate; In 1,2-dimethoxyethane; dichloromethane;
DOI:10.1021/acs.orglett.7b00796