(N,N-dimethylcarbamoyl)methylene bis dihydrochloride

Base Information

Chemical Name:(N,N-dimethylcarbamoyl)methylene bis dihydrochloride
CAS No.:87589-45-5
Molecular Formula:C₂₀H₃₅N₃O₅*2ClH
Molecular Weight:470.437
Hs Code.:

(N,N-dimethylcarbamoyl)methylene bis<trans-4-(aminomethyl)cyclohexanecarboxylate> dihydrochloride

Synonyms:(N,N-dimethylcarbamoyl)methylene bis dihydrochloride

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Chemical Property of (N,N-dimethylcarbamoyl)methylene bis dihydrochloride

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Technology Process of (N,N-dimethylcarbamoyl)methylene bis dihydrochloride

There total 3 articles about (N,N-dimethylcarbamoyl)methylene bis dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 87589-44-4
(N,N-dimethylcarbamoyl)methylene bismethyl>cyclohexanecarboxylate>

: 87589-45-5
(N,N-dimethylcarbamoyl)methylene bis dihydrochloride

Guidance literature:: With hydrogenchloride; In ethyl acetate; for 2h;
DOI:10.1021/jm00154a004

Reference yield:

: 1197-18-8
trans-4-aminomethyl-cyclohexyl-carboxylic acid

: 87589-45-5
(N,N-dimethylcarbamoyl)methylene bis dihydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / NaOH / H₂O; 2-methyl-propan-2-ol / 18 h / Ambient temperature

2: Et₃N / dimethylformamide / 84 h / 50 °C

3: 38 percent / HCl(g) / ethyl acetate / 2 h

With hydrogenchloride; sodium hydroxide; triethylamine; In water; ethyl acetate; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/jm00154a004

Reference yield:

: 27687-14-5
trans 4-(tert-butyloxycarbonylamino)methylcyclohexanecarboxylic acid

: 87589-45-5
(N,N-dimethylcarbamoyl)methylene bis dihydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / dimethylformamide / 84 h / 50 °C

2: 38 percent / HCl(g) / ethyl acetate / 2 h

With hydrogenchloride; triethylamine; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm00154a004