phenyl 1,4-dizincbromide

Base Information

Chemical Name:phenyl 1,4-dizincbromide
CAS No.:301300-52-7
Molecular Formula:C₆H₄Br₂Zn₂
Molecular Weight:366.686
Hs Code.:

Synonyms:phenyl 1,4-dizincbromide

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Chemical Property of phenyl 1,4-dizincbromide

Chemical Property:

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Technology Process of phenyl 1,4-dizincbromide

There total 3 articles about phenyl 1,4-dizincbromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 106-37-6
1.4-dibromobenzene

: 7440-66-6
zinc

: 301300-52-7
phenyl 1,4-dizincbromide

: 521097-87-0
BrZnC₆H₄C₆H₄ZnBr

: 210407-20-8
4-bromophenylzinc bromide

Guidance literature:: With trifluoroacetic acid; cobalt(II) bromide; zinc dibromide; In acetonitrile; the mixt. in CH3CN was stirred at room temp., then thienylbromide was added, stirred at room temp.; GC analysis;
DOI:10.1021/ja0289494

Reference yield:

: 106-37-6
1.4-dibromobenzene

: 7440-66-6
zinc

: 301300-52-7
phenyl 1,4-dizincbromide

Guidance literature:: zinc; With para-bromotoluene; trifluoroacetic acid; cobalt(II) chloride; zinc dibromide; In acetonitrile; at 20 ℃; for 0.5h; Inert atmosphere; Schlenk technique;

1.4-dibromobenzene; In acetonitrile; at 20 ℃; for 3h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c3dt52596a

Reference yield:

: 106-37-6
1.4-dibromobenzene

: 7646-85-7,24359-56-6
zinc(II) chloride

: 301300-52-7
phenyl 1,4-dizincbromide

Guidance literature:: zinc(II) chloride; With iodine; magnesium; In tetrahydrofuran; Inert atmosphere;

1.4-dibromobenzene; In tetrahydrofuran; Inert atmosphere; Cooling with ice;
DOI:10.1039/c4ob00638k