10-(4-(hexyloxy)phenyl)-7-(10-(4-(hexyloxy)phenyl)-10H-phenothiazin-7-yl)-10H-phenothiazine-3-carbaldehyde

Base Information

Chemical Name:10-(4-(hexyloxy)phenyl)-7-(10-(4-(hexyloxy)phenyl)-10H-phenothiazin-7-yl)-10H-phenothiazine-3-carbaldehyde
CAS No.:1403613-85-3
Molecular Formula:C₄₉H₄₈N₂O₃S₂
Molecular Weight:777.064
Hs Code.:

Synonyms:10-(4-(hexyloxy)phenyl)-7-(10-(4-(hexyloxy)phenyl)-10H-phenothiazin-7-yl)-10H-phenothiazine-3-carbaldehyde

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Chemical Property of 10-(4-(hexyloxy)phenyl)-7-(10-(4-(hexyloxy)phenyl)-10H-phenothiazin-7-yl)-10H-phenothiazine-3-carbaldehyde

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Technology Process of 10-(4-(hexyloxy)phenyl)-7-(10-(4-(hexyloxy)phenyl)-10H-phenothiazin-7-yl)-10H-phenothiazine-3-carbaldehyde

There total 4 articles about 10-(4-(hexyloxy)phenyl)-7-(10-(4-(hexyloxy)phenyl)-10H-phenothiazin-7-yl)-10H-phenothiazine-3-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1403613-84-2
3-(3-bromo-10-(4-(hexyloxy)phenyl)-10H-phenothiazin-7-yl)-10-(4-(hexyloxy)phenyl)-10H-phenothiazine

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1403613-85-3
10-(4-(hexyloxy)phenyl)-7-(10-(4-(hexyloxy)phenyl)-10H-phenothiazin-7-yl)-10H-phenothiazine-3-carbaldehyde

Guidance literature:: 3-(3-bromo-10-(4-(hexyloxy)phenyl)-10H-phenothiazin-7-yl)-10-(4-(hexyloxy)phenyl)-10H-phenothiazine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

N,N-dimethyl-formamide; In tetrahydrofuran; hexane; at -78 ℃; for 6h; Inert atmosphere;
DOI:10.1039/c2jm35556f

Reference yield:

: {10-[4-(hexyloxy)phenyl]-10H-phenothiazin-3-yl}boronic acid

: 1403613-85-3
10-(4-(hexyloxy)phenyl)-7-(10-(4-(hexyloxy)phenyl)-10H-phenothiazin-7-yl)-10H-phenothiazine-3-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; water; toluene / 12 h / 60 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

2.2: 6 h / -78 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; potassium carbonate; In tetrahydrofuran; hexane; water; toluene; 1.1: |Suzuki-Miyaura Coupling;
DOI:10.1039/c2jm35556f

Reference yield:

: 1403613-81-9
3-bromo-10-[4-(hexyloxy)phenyl]-10H-phenothiazine

: 1403613-85-3
10-(4-(hexyloxy)phenyl)-7-(10-(4-(hexyloxy)phenyl)-10H-phenothiazin-7-yl)-10H-phenothiazine-3-carbaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 - 0 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: hydrogenchloride; water / tetrahydrofuran; hexane / 1 h / 20 °C / Inert atmosphere

3.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; water; toluene / 12 h / 60 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

4.2: 6 h / -78 °C / Inert atmosphere

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; water; potassium carbonate; In tetrahydrofuran; hexane; water; toluene; 3.1: |Suzuki-Miyaura Coupling;
DOI:10.1039/c2jm35556f