(S,Z)-2-((2-(4-(4-chlorobenzoyl)phenoxy)-2-methylpropanoyloxy) methoxy)-1-(2-(hydroxymethyl)pyrrolidin-1-yl)diazene oxide

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Chemical Name:(S,Z)-2-((2-(4-(4-chlorobenzoyl)phenoxy)-2-methylpropanoyloxy) methoxy)-1-(2-(hydroxymethyl)pyrrolidin-1-yl)diazene oxide
CAS No.:1609495-42-2
Molecular Formula:C₂₃H₂₆ClN₃O₇
Molecular Weight:491.928
Hs Code.:

Synonyms:(S,Z)-2-((2-(4-(4-chlorobenzoyl)phenoxy)-2-methylpropanoyloxy) methoxy)-1-(2-(hydroxymethyl)pyrrolidin-1-yl)diazene oxide

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Chemical Property of (S,Z)-2-((2-(4-(4-chlorobenzoyl)phenoxy)-2-methylpropanoyloxy) methoxy)-1-(2-(hydroxymethyl)pyrrolidin-1-yl)diazene oxide

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Technology Process of (S,Z)-2-((2-(4-(4-chlorobenzoyl)phenoxy)-2-methylpropanoyloxy) methoxy)-1-(2-(hydroxymethyl)pyrrolidin-1-yl)diazene oxide

There total 4 articles about (S,Z)-2-((2-(4-(4-chlorobenzoyl)phenoxy)-2-methylpropanoyloxy) methoxy)-1-(2-(hydroxymethyl)pyrrolidin-1-yl)diazene oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: (S,Z)-2-hydroxy-1-(2-(hydroxymethyl)pyrrolidin-1-yl)diazene oxide sodium salt

: 1609495-38-6
iodomethyl 2-(4-(4-chlorobenzoyl)phenoxy)-2-methylpropanoate

: 1609495-42-2
(S,Z)-2-((2-(4-(4-chlorobenzoyl)phenoxy)-2-methylpropanoyloxy) methoxy)-1-(2-(hydroxymethyl)pyrrolidin-1-yl)diazene oxide

Guidance literature:: In hexane; N,N-dimethyl-formamide; at 20 ℃; for 1.06667h; Cooling with ice;

Reference yield:

: 1094101-30-0
chloromethyl 2-(4-(4-chlorobenzoyl)phenoxy)-2-methylpropanoate

: 1609495-42-2
(S,Z)-2-((2-(4-(4-chlorobenzoyl)phenoxy)-2-methylpropanoyloxy) methoxy)-1-(2-(hydroxymethyl)pyrrolidin-1-yl)diazene oxide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium iodide / acetone / 6.17 h / 20 - 50 °C

2: N,N-dimethyl-formamide; hexane / 1.07 h / 20 °C / Cooling with ice

With sodium iodide; In hexane; N,N-dimethyl-formamide; acetone;

Reference yield:

: 42017-89-0
fenofibric acid

: 1609495-42-2
(S,Z)-2-((2-(4-(4-chlorobenzoyl)phenoxy)-2-methylpropanoyloxy) methoxy)-1-(2-(hydroxymethyl)pyrrolidin-1-yl)diazene oxide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogencarbonate; tetra(n-butyl)ammonium hydrogensulfate / water / 0.25 h / 20 °C

1.2: 20 °C / Cooling with ice

2.1: sodium iodide / acetone / 6.17 h / 20 - 50 °C

3.1: N,N-dimethyl-formamide; hexane / 1.07 h / 20 °C / Cooling with ice

With tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; sodium iodide; In hexane; water; N,N-dimethyl-formamide; acetone;