tert-butyl((1R,5R,6S)-5-((S)-5-(4-methoxybenzyloxy)-4-methylpent-1-en-2-yl)-2,6-dimethylcyclohex-2-enyloxy)diphenylsilane

Base Information

Chemical Name:tert-butyl((1R,5R,6S)-5-((S)-5-(4-methoxybenzyloxy)-4-methylpent-1-en-2-yl)-2,6-dimethylcyclohex-2-enyloxy)diphenylsilane
CAS No.:1030607-33-0
Molecular Formula:C₃₈H₅₀O₃Si
Molecular Weight:582.899
Hs Code.:

Synonyms:tert-butyl((1R,5R,6S)-5-((S)-5-(4-methoxybenzyloxy)-4-methylpent-1-en-2-yl)-2,6-dimethylcyclohex-2-enyloxy)diphenylsilane

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Chemical Property of tert-butyl((1R,5R,6S)-5-((S)-5-(4-methoxybenzyloxy)-4-methylpent-1-en-2-yl)-2,6-dimethylcyclohex-2-enyloxy)diphenylsilane

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Technology Process of tert-butyl((1R,5R,6S)-5-((S)-5-(4-methoxybenzyloxy)-4-methylpent-1-en-2-yl)-2,6-dimethylcyclohex-2-enyloxy)diphenylsilane

There total 1 articles about tert-butyl((1R,5R,6S)-5-((S)-5-(4-methoxybenzyloxy)-4-methylpent-1-en-2-yl)-2,6-dimethylcyclohex-2-enyloxy)diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1030607-34-1
1-((1R,5R,6S)-5-(tert-butyldiphenylsilyloxy)-4,6-dimethylcyclohex-3-enyl)vinyl trifluoromethanesulfonate

: 183894-33-9
(R)-(+)-1-[(3'-iodo-2'-methylpropoxy)methyl]-4-methoxybenzene

: 1030607-33-0
tert-butyl((1R,5R,6S)-5-((S)-5-(4-methoxybenzyloxy)-4-methylpent-1-en-2-yl)-2,6-dimethylcyclohex-2-enyloxy)diphenylsilane

Guidance literature:: (R)-(+)-1-[(3'-iodo-2'-methylpropoxy)methyl]-4-methoxybenzene; With tert.-butyl lithium; zinc(II) chloride; In tetrahydrofuran; pentane; at -78 - 20 ℃; for 1.58333h; Inert atmosphere;

1-((1R,5R,6S)-5-(tert-butyldiphenylsilyloxy)-4,6-dimethylcyclohex-3-enyl)vinyl trifluoromethanesulfonate; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; lithium chloride; In tetrahydrofuran; pentane; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol800419v

Reference yield:

: 1030607-33-0
tert-butyl((1R,5R,6S)-5-((S)-5-(4-methoxybenzyloxy)-4-methylpent-1-en-2-yl)-2,6-dimethylcyclohex-2-enyloxy)diphenylsilane

: C₃₈H₅₄O₇Si

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; osmium(VIII) oxide; potassium carbonate; potassium hexacyanoferrate(III); In water; tert-butyl alcohol; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1021/ol800419v