1-((1R,5R,6S)-5-(tert-butyldiphenylsilyloxy)-4,6-dimethylcyclohex-3-enyl)vinyl trifluoromethanesulfonate

Base Information

Chemical Name:1-((1R,5R,6S)-5-(tert-butyldiphenylsilyloxy)-4,6-dimethylcyclohex-3-enyl)vinyl trifluoromethanesulfonate
CAS No.:1030607-34-1
Molecular Formula:C₂₇H₃₃F₃O₄SSi
Molecular Weight:538.703
Hs Code.:

Synonyms:1-((1R,5R,6S)-5-(tert-butyldiphenylsilyloxy)-4,6-dimethylcyclohex-3-enyl)vinyl trifluoromethanesulfonate

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Chemical Property of 1-((1R,5R,6S)-5-(tert-butyldiphenylsilyloxy)-4,6-dimethylcyclohex-3-enyl)vinyl trifluoromethanesulfonate

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Technology Process of 1-((1R,5R,6S)-5-(tert-butyldiphenylsilyloxy)-4,6-dimethylcyclohex-3-enyl)vinyl trifluoromethanesulfonate

There total 1 articles about 1-((1R,5R,6S)-5-(tert-butyldiphenylsilyloxy)-4,6-dimethylcyclohex-3-enyl)vinyl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1030607-39-6
1-((1R,5R,6S)-5-(tert-butyldiphenylsilyloxy)-4,6-dimethylcyclohex-3-enyl)ethanone

: 145100-51-2
N-(5-chloropyridin-2-yl)-1,1,1-trifluoro-N-[(trifluoromethyl)sulphonyl]methanesulphonamide

: 1030607-34-1
1-((1R,5R,6S)-5-(tert-butyldiphenylsilyloxy)-4,6-dimethylcyclohex-3-enyl)vinyl trifluoromethanesulfonate

Guidance literature:: 1-((1R,5R,6S)-5-(tert-butyldiphenylsilyloxy)-4,6-dimethylcyclohex-3-enyl)ethanone; With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 1.5h; Inert atmosphere;

N-(5-chloropyridin-2-yl)-1,1,1-trifluoro-N-[(trifluoromethyl)sulphonyl]methanesulphonamide; With N,N,N,N,N,N-hexamethylphosphoric triamide; In tetrahydrofuran; at -78 - 0 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol800419v

Reference yield: 86.0%

: 1030607-34-1
1-((1R,5R,6S)-5-(tert-butyldiphenylsilyloxy)-4,6-dimethylcyclohex-3-enyl)vinyl trifluoromethanesulfonate

: 183894-33-9
(R)-(+)-1-[(3'-iodo-2'-methylpropoxy)methyl]-4-methoxybenzene

: 1030607-33-0
tert-butyl((1R,5R,6S)-5-((S)-5-(4-methoxybenzyloxy)-4-methylpent-1-en-2-yl)-2,6-dimethylcyclohex-2-enyloxy)diphenylsilane

Guidance literature:: (R)-(+)-1-[(3'-iodo-2'-methylpropoxy)methyl]-4-methoxybenzene; With tert.-butyl lithium; zinc(II) chloride; In tetrahydrofuran; pentane; at -78 - 20 ℃; for 1.58333h; Inert atmosphere;

1-((1R,5R,6S)-5-(tert-butyldiphenylsilyloxy)-4,6-dimethylcyclohex-3-enyl)vinyl trifluoromethanesulfonate; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; lithium chloride; In tetrahydrofuran; pentane; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol800419v