(6S,9S)-S-4-nitrophenyl 6,9-dibenzyl-2,2-dimethyl-4,7,10-trioxo-3-oxa-5,8,11-triazatridecane-13-thioate

Base Information

• Chemical Name: (6S,9S)-S-4-nitrophenyl 6,9-dibenzyl-2,2-dimethyl-4,7,10-trioxo-3-oxa-5,8,11-triazatridecane-13-thioate
• CAS No.: 1620161-82-1
• Molecular Formula: C₃₁H₃₄N₄O₇S
• Molecular Weight: 606.7

Synonyms:(6S,9S)-S-4-nitrophenyl 6,9-dibenzyl-2,2-dimethyl-4,7,10-trioxo-3-oxa-5,8,11-triazatridecane-13-thioate

Chemical Property of (6S,9S)-S-4-nitrophenyl 6,9-dibenzyl-2,2-dimethyl-4,7,10-trioxo-3-oxa-5,8,11-triazatridecane-13-thioate

Chemical Property:

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Technology Process of (6S,9S)-S-4-nitrophenyl 6,9-dibenzyl-2,2-dimethyl-4,7,10-trioxo-3-oxa-5,8,11-triazatridecane-13-thioate

There total 1 articles about (6S,9S)-S-4-nitrophenyl 6,9-dibenzyl-2,2-dimethyl-4,7,10-trioxo-3-oxa-5,8,11-triazatridecane-13-thioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

N-tert-butoxycarbonyl-L-phenylalanine-L-phenylalanine-glycine (82816-76-0) + para-nitrobenzenethiol (1849-36-1) → (6S,9S)-S-4-nitrophenyl 6,9-dibenzyl-2,2-dimethyl-4,7,10-trioxo-3-oxa-5,8,11-triazatridecane-13-thioate (1620161-82-1)

Guidance literature:

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

DOI:10.1021/ol501669n

Reference yield: 89.0%

L-arginine methyl ester (2577-94-8,65160-70-5) + (6S,9S)-S-4-nitrophenyl 6,9-dibenzyl-2,2-dimethyl-4,7,10-trioxo-3-oxa-5,8,11-triazatridecane-13-thioate (1620161-82-1) → (6S,9S,15S)-methyl 6,9-dibenzyl-15-(3-guanidinopropyl)-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate (1620161-87-6)

Guidance literature:

With sodium hydrogencarbonate; In dimethyl sulfoxide; at 20 ℃; for 25h; Inert atmosphere;

DOI:10.1021/ol501669n

Reference yield: 72.0%

(6S,9S)-S-4-nitrophenyl 6,9-dibenzyl-2,2-dimethyl-4,7,10-trioxo-3-oxa-5,8,11-triazatridecane-13-thioate (1620161-82-1) + L-serine benzyl ester → (6S,9S,15S)-benzyl 6,9-dibenzyl-15-(hydroxymethyl)-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate (1620161-86-5)

Guidance literature:

With sodium hydrogencarbonate; In dimethyl sulfoxide; at 20 ℃; for 25h; Inert atmosphere;

DOI:10.1021/ol501669n

upstream raw materials:

N-tert-butoxycarbonyl-L-phenylalanine-L-phenylalanine-glycine

para-nitrobenzenethiol

Downstream raw materials:

(6S,9S,15S)-tert-butyl 15-(3-amino-3-oxopropyl)-6,9-dibenzyl-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate

(6S,9S,15S)-benzyl 6,9-dibenzyl-15-(4-hydroxybenzyl)-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate

(6S,9S,15S)-6,9-dibenzyl-15-((benzyloxy)carbonyl)-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazaheptadecan-17-oic acid

(6S,9S,15S)-benzyl 6,9-dibenzyl-15-(hydroxymethyl)-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate

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