(6S,9S,15S)-methyl 6,9-dibenzyl-15-(3-guanidinopropyl)-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate

Base Information

Chemical Name:(6S,9S,15S)-methyl 6,9-dibenzyl-15-(3-guanidinopropyl)-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate
CAS No.:1620161-87-6
Molecular Formula:C₃₂H₄₅N₇O₇
Molecular Weight:639.752
Hs Code.:

Synonyms:(6S,9S,15S)-methyl 6,9-dibenzyl-15-(3-guanidinopropyl)-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate

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Chemical Property of (6S,9S,15S)-methyl 6,9-dibenzyl-15-(3-guanidinopropyl)-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate

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Technology Process of (6S,9S,15S)-methyl 6,9-dibenzyl-15-(3-guanidinopropyl)-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate

There total 2 articles about (6S,9S,15S)-methyl 6,9-dibenzyl-15-(3-guanidinopropyl)-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 2577-94-8,65160-70-5
L-arginine methyl ester

: 1620161-82-1
(6S,9S)-S-4-nitrophenyl 6,9-dibenzyl-2,2-dimethyl-4,7,10-trioxo-3-oxa-5,8,11-triazatridecane-13-thioate

: 1620161-87-6
(6S,9S,15S)-methyl 6,9-dibenzyl-15-(3-guanidinopropyl)-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate

Guidance literature:: With sodium hydrogencarbonate; In dimethyl sulfoxide; at 20 ℃; for 25h; Inert atmosphere;
DOI:10.1021/ol501669n

Reference yield:

: 82816-76-0
N-tert-butoxycarbonyl-L-phenylalanine-L-phenylalanine-glycine

: 1620161-87-6
(6S,9S,15S)-methyl 6,9-dibenzyl-15-(3-guanidinopropyl)-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2: sodium hydrogencarbonate / dimethyl sulfoxide / 25 h / 20 °C / Inert atmosphere

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ol501669n