3-Chloro-N-(diphenyl-phosphinoylmethyl)-N-(4-methoxy-benzyl)-isonicotinamide

Base Information

Chemical Name:3-Chloro-N-(diphenyl-phosphinoylmethyl)-N-(4-methoxy-benzyl)-isonicotinamide
CAS No.:195005-10-8
Molecular Formula:C₂₇H₂₄ClN₂O₃P
Molecular Weight:490.926
Hs Code.:

Synonyms:3-Chloro-N-(diphenyl-phosphinoylmethyl)-N-(4-methoxy-benzyl)-isonicotinamide

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Chemical Property of 3-Chloro-N-(diphenyl-phosphinoylmethyl)-N-(4-methoxy-benzyl)-isonicotinamide

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Technology Process of 3-Chloro-N-(diphenyl-phosphinoylmethyl)-N-(4-methoxy-benzyl)-isonicotinamide

There total 1 articles about 3-Chloro-N-(diphenyl-phosphinoylmethyl)-N-(4-methoxy-benzyl)-isonicotinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 88912-27-0
3-chloro-isonicotinic acid

: 195005-12-0
N-[(diphenylphosphinoyl)methyl]-N-(4-methoxybenzyl)amine

: 195005-10-8
3-Chloro-N-(diphenyl-phosphinoylmethyl)-N-(4-methoxy-benzyl)-isonicotinamide

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1016/S0040-4020(97)00680-7

Reference yield: 69.0%

: 195005-10-8
3-Chloro-N-(diphenyl-phosphinoylmethyl)-N-(4-methoxy-benzyl)-isonicotinamide

: 3-(Diphenyl-phosphinoyl)-2-(4-methoxy-benzyl)-2,3-dihydro-pyrrolo[3,4-c]pyridin-1-one

Guidance literature:: With potassium hexamethylsilazane; In tetrahydrofuran; toluene; 1.) -78 deg C, 0.25 h, 2.) -78 deg C -> room temperature, 2 h;
DOI:10.1016/S0040-4020(97)00680-7

Reference yield:

: 78-84-2
isobutyraldehyde

: 195005-10-8
3-Chloro-N-(diphenyl-phosphinoylmethyl)-N-(4-methoxy-benzyl)-isonicotinamide

: 2-(4-Methoxy-benzyl)-3-[2-methyl-prop-(E)-ylidene]-2,3-dihydro-pyrrolo[3,4-c]pyridin-1-one

: 2-(4-Methoxy-benzyl)-3-[2-methyl-prop-(E)-ylidene]-2,3-dihydro-pyrrolo[3,4-c]pyridin-1-one

Guidance literature:: With potassium hexamethylsilazane; Yield given. Multistep reaction. Yields of byproduct given; 1.) toluene, THF, -78 deg C -> room temperature, 2 h, 2.) THF, -30 deg C -> room temperature, 0.5 h;
DOI:10.1016/S0040-4020(97)00680-7