(1R,5R,6S)-6-(2-hydroxyethyl)-3-methyl-5-(prop-1-en-2-yl)cyclohex-2-enol

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Chemical Name:(1R,5R,6S)-6-(2-hydroxyethyl)-3-methyl-5-(prop-1-en-2-yl)cyclohex-2-enol
CAS No.:944450-09-3
Molecular Formula:C₁₂H₂₀O₂
Molecular Weight:196.29
Hs Code.:
Mol file:944450-09-3.mol

Synonyms:(1R,5R,6S)-6-(2-hydroxyethyl)-3-methyl-5-(prop-1-en-2-yl)cyclohex-2-enol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,5R,6S)-6-(2-hydroxyethyl)-3-methyl-5-(prop-1-en-2-yl)cyclohex-2-enol Edit

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Technology Process of (1R,5R,6S)-6-(2-hydroxyethyl)-3-methyl-5-(prop-1-en-2-yl)cyclohex-2-enol

There total 2 articles about (1R,5R,6S)-6-(2-hydroxyethyl)-3-methyl-5-(prop-1-en-2-yl)cyclohex-2-enol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 944450-08-2
ethyl 2-[(1S,6R)-4-methyl-2-oxo-6-(prop-1-en-2-yl)cyclohex-3-enyl]acetate

: 944450-09-3
(1R,5R,6S)-6-(2-hydroxyethyl)-3-methyl-5-(prop-1-en-2-yl)cyclohex-2-enol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at -78 - 20 ℃;
DOI:10.1021/jo070165r

Reference yield:

: 731811-34-0,731811-35-1
(-)-5-isopropenyl-3-methyl-cyclohex-2-enone

: 944450-09-3
(1R,5R,6S)-6-(2-hydroxyethyl)-3-methyl-5-(prop-1-en-2-yl)cyclohex-2-enol

Guidance literature:: Multi-step reaction with 2 steps

1.1: LiHMDS / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 85 percent / tetrahydrofuran; hexane / 4.75 h / -78 - 20 °C

2.1: 72 percent / lithium aluminum hydride / diethyl ether / -78 - 20 °C

With lithium aluminium tetrahydride; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1021/jo070165r