4,4'-Bis(p-1,4,7,10-tetraoxa-13-azacyclopentadecan-13-ylstyryl)-2,2'-bipyridine

Base Information

Chemical Name:4,4'-Bis(p-1,4,7,10-tetraoxa-13-azacyclopentadecan-13-ylstyryl)-2,2'-bipyridine
CAS No.:138473-69-5
Molecular Formula:C₄₆H₅₈N₄O₈
Molecular Weight:794.989
Hs Code.:

Synonyms:4,4'-Bis(p-1,4,7,10-tetraoxa-13-azacyclopentadecan-13-ylstyryl)-2,2'-bipyridine

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Chemical Property of 4,4'-Bis(p-1,4,7,10-tetraoxa-13-azacyclopentadecan-13-ylstyryl)-2,2'-bipyridine

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Technology Process of 4,4'-Bis(p-1,4,7,10-tetraoxa-13-azacyclopentadecan-13-ylstyryl)-2,2'-bipyridine

There total 2 articles about 4,4'-Bis(p-1,4,7,10-tetraoxa-13-azacyclopentadecan-13-ylstyryl)-2,2'-bipyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 4,4'-Bis-<2-hydroxy-2-p-(1,4,7,10-tetraoxa-13-azacyclopentadecan-13-ylphenyl)ethyl>-2,2'-bipyridine

: 138473-69-5
4,4'-Bis(p-1,4,7,10-tetraoxa-13-azacyclopentadecan-13-ylstyryl)-2,2'-bipyridine

Guidance literature:: With pyridinium p-toluenesulfonate; In toluene; Heating;
DOI:10.1039/DT9930002629

Reference yield:

: 1134-35-6
4,4'-dimethyl-2,2'-bipyridines

: 66749-96-0
4-(1,4,7,10-tetraoxa-13-aza-cyclopentadec-13-yl)-benzaldehyde

: 138473-69-5
4,4'-Bis(p-1,4,7,10-tetraoxa-13-azacyclopentadecan-13-ylstyryl)-2,2'-bipyridine

Guidance literature:: Yield given. Multistep reaction;
DOI:10.1039/c39910001460

Reference yield:

: ammonium hexafluorophosphate

: 14898-67-0
ruthenium(III) chloride trihydrate

: 138473-69-5
4,4'-Bis(p-1,4,7,10-tetraoxa-13-azacyclopentadecan-13-ylstyryl)-2,2'-bipyridine

: Ru⁽²⁺⁾*3(C₅H₃NCHCHC₆H₄C₁₀H₂₀NO₄)2*2PF₆^(1-)={Ru((C₅H₃NCHCHC₆H₄C₁₀H₂₀NO₄)2)3}{PF₆}2

Guidance literature:: In N,N-dimethyl-formamide; soln. of ligand and Ru salt refluxed; purifn. on Sephadex LH-20, addn. of NH4PF6, pptn.;
DOI:10.1039/c39910001460