2,3,4,6-tetra-O-benzyl-1-O-[((p-nitrobenzoyl)sulfanyl)thiocarbonyl]-α-D-galactopyranose

Base Information

Chemical Name:2,3,4,6-tetra-O-benzyl-1-O-[((p-nitrobenzoyl)sulfanyl)thiocarbonyl]-α-D-galactopyranose
CAS No.:405060-35-7
Molecular Formula:C₄₂H₃₉NO₉S₂
Molecular Weight:765.905
Hs Code.:

Synonyms:2,3,4,6-tetra-O-benzyl-1-O-[((p-nitrobenzoyl)sulfanyl)thiocarbonyl]-α-D-galactopyranose

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Chemical Property of 2,3,4,6-tetra-O-benzyl-1-O-[((p-nitrobenzoyl)sulfanyl)thiocarbonyl]-α-D-galactopyranose

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Technology Process of 2,3,4,6-tetra-O-benzyl-1-O-[((p-nitrobenzoyl)sulfanyl)thiocarbonyl]-α-D-galactopyranose

There total 2 articles about 2,3,4,6-tetra-O-benzyl-1-O-[((p-nitrobenzoyl)sulfanyl)thiocarbonyl]-α-D-galactopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6386-24-9
2,3,4,6-tetra-O-benzyl-D-galactopyranose

: 405060-35-7
2,3,4,6-tetra-O-benzyl-1-O-[((p-nitrobenzoyl)sulfanyl)thiocarbonyl]-α-D-galactopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / tetrahydrofuran / 0 °C

2: 2 h / 0 °C

With sodium hydride; In tetrahydrofuran;
DOI:10.1016/S0040-4039(01)02122-0

Reference yield:

: 122-04-3
4-nitro-benzoyl chloride

: C₃₅H₃₅O₆S₂^(1-)*Na⁽¹⁺⁾

: 405060-36-8
C₄₂H₃₉NO₉S₂

: 405060-35-7
2,3,4,6-tetra-O-benzyl-1-O-[((p-nitrobenzoyl)sulfanyl)thiocarbonyl]-α-D-galactopyranose

Guidance literature:: at 0 ℃; for 2h;
DOI:10.1016/S0040-4039(01)02122-0

Reference yield: 85.0%

: 405060-35-7
2,3,4,6-tetra-O-benzyl-1-O-[((p-nitrobenzoyl)sulfanyl)thiocarbonyl]-α-D-galactopyranose

: 405060-39-1
2,3,4,6-tetra-O-benzyl-1-deoxy-1-thio-α-D-galactopyranose

Guidance literature:: With 1H-imidazole; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 20 ℃; for 1.5h;
DOI:10.1016/S0040-4039(01)02122-0