tris{5-[(4'-methoxyphenyl)methoxymethyl]-1-methyl-1H-2-imidazolyl}methyl methyl ether

Base Information

Chemical Name:tris{5-[(4'-methoxyphenyl)methoxymethyl]-1-methyl-1H-2-imidazolyl}methyl methyl ether
CAS No.:384821-16-3
Molecular Formula:C₄₁H₄₈N₆O₇
Molecular Weight:736.868
Hs Code.:

Synonyms:tris{5-[(4'-methoxyphenyl)methoxymethyl]-1-methyl-1H-2-imidazolyl}methyl methyl ether

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Chemical Property of tris{5-[(4'-methoxyphenyl)methoxymethyl]-1-methyl-1H-2-imidazolyl}methyl methyl ether

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Technology Process of tris{5-[(4'-methoxyphenyl)methoxymethyl]-1-methyl-1H-2-imidazolyl}methyl methyl ether

There total 4 articles about tris{5-[(4'-methoxyphenyl)methoxymethyl]-1-methyl-1H-2-imidazolyl}methyl methyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 384821-15-2
tris{5-[(4'-methoxyphenyl)methoxymethyl]-1-methyl-1H-2-imidazolyl}methyl alcohol

: 74-88-4
methyl iodide

: 384821-16-3
tris{5-[(4'-methoxyphenyl)methoxymethyl]-1-methyl-1H-2-imidazolyl}methyl methyl ether

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/jo010737m

Reference yield:

: 38993-84-9
(1-methyl-1H-imidazol-5-yl)methanol

: 384821-16-3
tris{5-[(4'-methoxyphenyl)methoxymethyl]-1-methyl-1H-2-imidazolyl}methyl methyl ether

Guidance literature:: Multi-step reaction with 3 steps

1.1: 61 percent / NaH / dimethylformamide / 20 °C

2.1: n-BuLi / tetrahydrofuran; hexane / 1 h / -78 - -40 °C

2.2: 77 percent / tetrahydrofuran / 24 h / -78 - 20 °C

3.1: 73 percent / NaH / tetrahydrofuran / 20 °C

With n-butyllithium; sodium hydride; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1021/jo010737m

Reference yield:

: 143122-18-3
5-hydroxymethyl-2-mercapto-1-methyl-1H-imidazole

: 384821-16-3
tris{5-[(4'-methoxyphenyl)methoxymethyl]-1-methyl-1H-2-imidazolyl}methyl methyl ether

Guidance literature:: Multi-step reaction with 4 steps

1.1: 75 percent / aq. HNO₃; NaNO₂ / 20 °C

2.1: 61 percent / NaH / dimethylformamide / 20 °C

3.1: n-BuLi / tetrahydrofuran; hexane / 1 h / -78 - -40 °C

3.2: 77 percent / tetrahydrofuran / 24 h / -78 - 20 °C

4.1: 73 percent / NaH / tetrahydrofuran / 20 °C

With n-butyllithium; nitric acid; sodium hydride; sodium nitrite; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1021/jo010737m