5-(2,6-bis(2-(2-(2-(3-(benzyloxy)-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)-5-tertbutylbenzyl)-4-tert-butylphenoxy)-N-(benzyloxy)pentanamide

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Chemical Name:5-(2,6-bis(2-(2-(2-(3-(benzyloxy)-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)-5-tertbutylbenzyl)-4-tert-butylphenoxy)-N-(benzyloxy)pentanamide
CAS No.:1407969-01-0
Molecular Formula:C₇₆H₉₁N₃O₁₁
Molecular Weight:1222.57
Hs Code.:

Synonyms:5-(2,6-bis(2-(2-(2-(3-(benzyloxy)-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)-5-tertbutylbenzyl)-4-tert-butylphenoxy)-N-(benzyloxy)pentanamide

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Chemical Property of 5-(2,6-bis(2-(2-(2-(3-(benzyloxy)-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)-5-tertbutylbenzyl)-4-tert-butylphenoxy)-N-(benzyloxy)pentanamide

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Technology Process of 5-(2,6-bis(2-(2-(2-(3-(benzyloxy)-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)-5-tertbutylbenzyl)-4-tert-butylphenoxy)-N-(benzyloxy)pentanamide

There total 7 articles about 5-(2,6-bis(2-(2-(2-(3-(benzyloxy)-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)-5-tertbutylbenzyl)-4-tert-butylphenoxy)-N-(benzyloxy)pentanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆₉H₈₃ClN₂O₁₀

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 1407969-01-0
5-(2,6-bis(2-(2-(2-(3-(benzyloxy)-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)-5-tertbutylbenzyl)-4-tert-butylphenoxy)-N-(benzyloxy)pentanamide

Guidance literature:: O-benzylhydoxylamine hydrochloride; With triethylamine; In dichloromethane; at 0 - 20 ℃; for 0.75h; Inert atmosphere;

C₆₉H₈₃ClN₂O₁₀; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.tet.2012.09.032

Reference yield:

: C₆₉H₈₄N₂O₁₁

: 1407969-01-0
5-(2,6-bis(2-(2-(2-(3-(benzyloxy)-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)-5-tertbutylbenzyl)-4-tert-butylphenoxy)-N-(benzyloxy)pentanamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl dichloride / benzene / 18 h / 20 °C

2.1: triethylamine / dichloromethane / 0.75 h / 0 - 20 °C / Inert atmosphere

2.2: 24 h / 20 °C / Inert atmosphere

With oxalyl dichloride; triethylamine; In dichloromethane; benzene;
DOI:10.1016/j.tet.2012.09.032

Reference yield:

: 1407968-98-2
ethyl 5-(2,6-bis(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-4-tert-butylphenoxy)pentanoate

: 1407969-01-0
5-(2,6-bis(2-(2-(2-(3-(benzyloxy)-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)-5-tertbutylbenzyl)-4-tert-butylphenoxy)-N-(benzyloxy)pentanamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 18 h / 20 - 70 °C / Inert atmosphere

3.1: lithium hydroxide / ethanol / 24 h / 20 °C

4.1: oxalyl dichloride / benzene / 18 h / 20 °C

5.1: triethylamine / dichloromethane / 0.75 h / 0 - 20 °C / Inert atmosphere

5.2: 24 h / 20 °C / Inert atmosphere

With oxalyl dichloride; tetrabutyl ammonium fluoride; caesium carbonate; triethylamine; lithium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1016/j.tet.2012.09.032