5-(2,6-bis(5-tert-butyl-2-(2-(2-(3-hydroxy-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)benzyl)-4-tert-butylphenoxy)-N-hydroxypentanamide

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Chemical Name:5-(2,6-bis(5-tert-butyl-2-(2-(2-(3-hydroxy-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)benzyl)-4-tert-butylphenoxy)-N-hydroxypentanamide
CAS No.:1407969-02-1
Molecular Formula:C₅₅H₇₃N₃O₁₁
Molecular Weight:952.198
Hs Code.:

Synonyms:5-(2,6-bis(5-tert-butyl-2-(2-(2-(3-hydroxy-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)benzyl)-4-tert-butylphenoxy)-N-hydroxypentanamide

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Chemical Property of 5-(2,6-bis(5-tert-butyl-2-(2-(2-(3-hydroxy-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)benzyl)-4-tert-butylphenoxy)-N-hydroxypentanamide

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Technology Process of 5-(2,6-bis(5-tert-butyl-2-(2-(2-(3-hydroxy-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)benzyl)-4-tert-butylphenoxy)-N-hydroxypentanamide

There total 8 articles about 5-(2,6-bis(5-tert-butyl-2-(2-(2-(3-hydroxy-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)benzyl)-4-tert-butylphenoxy)-N-hydroxypentanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.9%

: 1407969-01-0
5-(2,6-bis(2-(2-(2-(3-(benzyloxy)-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)-5-tertbutylbenzyl)-4-tert-butylphenoxy)-N-(benzyloxy)pentanamide

: 1407969-02-1
5-(2,6-bis(5-tert-butyl-2-(2-(2-(3-hydroxy-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)benzyl)-4-tert-butylphenoxy)-N-hydroxypentanamide

Guidance literature:: With 10% Pd/C; hydrogen; In ethanol; at 20 ℃; for 48h;
DOI:10.1016/j.tet.2012.09.032

Reference yield:

: 1407969-00-9
ethyl 5-(2,6-bis(2-(2-(2-(3-(benzyloxy)-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)-5-tertbutylbenzyl)-4-tert-butylphenoxy)pentanoate

: 1407969-02-1
5-(2,6-bis(5-tert-butyl-2-(2-(2-(3-hydroxy-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)benzyl)-4-tert-butylphenoxy)-N-hydroxypentanamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium hydroxide / ethanol / 24 h / 20 °C

2.1: oxalyl dichloride / benzene / 18 h / 20 °C

3.1: triethylamine / dichloromethane / 0.75 h / 0 - 20 °C / Inert atmosphere

3.2: 24 h / 20 °C / Inert atmosphere

4.1: 10% Pd/C; hydrogen / ethanol / 48 h / 20 °C

With oxalyl dichloride; 10% Pd/C; hydrogen; triethylamine; lithium hydroxide; In ethanol; dichloromethane; benzene;
DOI:10.1016/j.tet.2012.09.032

Reference yield:

: C₆₉H₈₄N₂O₁₁

: 1407969-02-1
5-(2,6-bis(5-tert-butyl-2-(2-(2-(3-hydroxy-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)benzyl)-4-tert-butylphenoxy)-N-hydroxypentanamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: oxalyl dichloride / benzene / 18 h / 20 °C

2.1: triethylamine / dichloromethane / 0.75 h / 0 - 20 °C / Inert atmosphere

2.2: 24 h / 20 °C / Inert atmosphere

3.1: 10% Pd/C; hydrogen / ethanol / 48 h / 20 °C

With oxalyl dichloride; 10% Pd/C; hydrogen; triethylamine; In ethanol; dichloromethane; benzene;
DOI:10.1016/j.tet.2012.09.032