4-methoxy-N-(2-(4-methoxyphenyl)-1-methyl-4-oxo-1,4-dihydroquinolin-3-yl)benzamide

Base Information

Chemical Name:4-methoxy-N-(2-(4-methoxyphenyl)-1-methyl-4-oxo-1,4-dihydroquinolin-3-yl)benzamide
CAS No.:1309362-45-5
Molecular Formula:C₂₅H₂₂N₂O₄
Molecular Weight:414.461
Hs Code.:

Synonyms:4-methoxy-N-(2-(4-methoxyphenyl)-1-methyl-4-oxo-1,4-dihydroquinolin-3-yl)benzamide

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Chemical Property of 4-methoxy-N-(2-(4-methoxyphenyl)-1-methyl-4-oxo-1,4-dihydroquinolin-3-yl)benzamide

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Technology Process of 4-methoxy-N-(2-(4-methoxyphenyl)-1-methyl-4-oxo-1,4-dihydroquinolin-3-yl)benzamide

There total 2 articles about 4-methoxy-N-(2-(4-methoxyphenyl)-1-methyl-4-oxo-1,4-dihydroquinolin-3-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 876460-09-2
3-iodo-2-(4'-methoxyphenyl)-1-methylquinolin-4(1H)-one

: 3424-93-9
4-methoxyphenylacetamide

: 1309362-45-5
4-methoxy-N-(2-(4-methoxyphenyl)-1-methyl-4-oxo-1,4-dihydroquinolin-3-yl)benzamide

: 246181-55-5
1-methyl-2-(4’-methoxyphenyl)-1H-4-quinolone

Guidance literature:: With copper; potassium carbonate; N,N`-dimethylethylenediamine; In toluene; at 135 ℃; for 5h; Inert atmosphere;
DOI:10.1021/jo200680j

Reference yield:

: 882866-44-6
3-iodo-2-(4'-methoxyphenyl)-quinolin-4(1H)-one

: 1309362-45-5
4-methoxy-N-(2-(4-methoxyphenyl)-1-methyl-4-oxo-1,4-dihydroquinolin-3-yl)benzamide

: 246181-55-5
1-methyl-2-(4’-methoxyphenyl)-1H-4-quinolone

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / Inert atmosphere

1.2: 2 h / 20 °C / Inert atmosphere

2.1: copper; potassium carbonate; N,N`-dimethylethylenediamine / toluene / 5 h / 135 °C / Inert atmosphere

With copper; sodium hydride; potassium carbonate; N,N`-dimethylethylenediamine; In tetrahydrofuran; toluene; mineral oil; 2.1: Ullmann type reaction;
DOI:10.1021/jo200680j