phenyl 1-(3-(biphenyl-4-yloxy)-3-oxoprop-1-enyl)pyrrolidine-2-carboxylate

Base Information

Chemical Name:phenyl 1-(3-(biphenyl-4-yloxy)-3-oxoprop-1-enyl)pyrrolidine-2-carboxylate
CAS No.:1384256-83-0
Molecular Formula:C₂₆H₂₃NO₄
Molecular Weight:413.473
Hs Code.:

Synonyms:phenyl 1-(3-(biphenyl-4-yloxy)-3-oxoprop-1-enyl)pyrrolidine-2-carboxylate

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Chemical Property of phenyl 1-(3-(biphenyl-4-yloxy)-3-oxoprop-1-enyl)pyrrolidine-2-carboxylate

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Technology Process of phenyl 1-(3-(biphenyl-4-yloxy)-3-oxoprop-1-enyl)pyrrolidine-2-carboxylate

There total 6 articles about phenyl 1-(3-(biphenyl-4-yloxy)-3-oxoprop-1-enyl)pyrrolidine-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: biphenyl-4-yl propiolate

: phenyl pyrrolidine-2-carboxylate

: 1384256-83-0
phenyl 1-(3-(biphenyl-4-yloxy)-3-oxoprop-1-enyl)pyrrolidine-2-carboxylate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1039/c2cc32373g

Reference yield:

: 64411-39-8
1-tert-butyl 2-phenyl pyrrolidine-1,2-dicarboxylate

: 1384256-83-0
phenyl 1-(3-(biphenyl-4-yloxy)-3-oxoprop-1-enyl)pyrrolidine-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 1 h / 0 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C / Inert atmosphere

With N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c2cc32373g

Reference yield:

: 1384256-76-1
biphenyl-4-yl 3-(piperidin-1-yl)acrylate

: 1384256-83-0
phenyl 1-(3-(biphenyl-4-yloxy)-3-oxoprop-1-enyl)pyrrolidine-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: Irradiation

2: dmap; dicyclohexyl-carbodiimide / diethyl ether / 12 h / 20 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C / Inert atmosphere

With dmap; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; diethyl ether; 2: Steglich esterification;
DOI:10.1039/c2cc32373g