N-(2,3-dimethylphenyl)piperazinium N-(2,3-dimethylphenyl)piperazine-1-carbodithioic acid

Base Information

Chemical Name:N-(2,3-dimethylphenyl)piperazinium N-(2,3-dimethylphenyl)piperazine-1-carbodithioic acid
CAS No.:1353311-99-5
Molecular Formula:C₁₂H₁₈N₂*C₁₃H₁₈N₂S₂
Molecular Weight:456.72
Hs Code.:

Synonyms:N-(2,3-dimethylphenyl)piperazinium N-(2,3-dimethylphenyl)piperazine-1-carbodithioic acid

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Chemical Property of N-(2,3-dimethylphenyl)piperazinium N-(2,3-dimethylphenyl)piperazine-1-carbodithioic acid

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Technology Process of N-(2,3-dimethylphenyl)piperazinium N-(2,3-dimethylphenyl)piperazine-1-carbodithioic acid

There total 1 articles about N-(2,3-dimethylphenyl)piperazinium N-(2,3-dimethylphenyl)piperazine-1-carbodithioic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 75-15-0,12122-00-8
carbon disulfide

: 1013-22-5
1-(2,3-dimethylphenyl)piperazine

: 1353311-99-5
N-(2,3-dimethylphenyl)piperazinium N-(2,3-dimethylphenyl)piperazine-1-carbodithioic acid

Guidance literature:: In methanol; at -0.16 ℃; for 4h;
DOI:10.1016/j.poly.2011.10.025

Reference yield: 67.5%

: 1353311-99-5
N-(2,3-dimethylphenyl)piperazinium N-(2,3-dimethylphenyl)piperazine-1-carbodithioic acid

: 1135-99-5
diphenyltin(IV) dichloride

: chlorodiphenylstannyl N-(2,3-dimethylphenyl)piperazine-1-carbodithioate

Guidance literature:: In toluene; byproducts: (CH3)2C6H3(C4H10N2)Cl; stoich. mixt. refluxed for 6-7 h with stirring; filtered off, evapd., recrystd. (MeOH/CHCl3), elem. anal.;
DOI:10.1016/j.poly.2011.10.025

Reference yield: 62.8%

: 1353311-99-5
N-(2,3-dimethylphenyl)piperazinium N-(2,3-dimethylphenyl)piperazine-1-carbodithioic acid

: 639-58-7
triphenyltin chloride

: 1353311-92-8
triphenylstannyl N-(2,3-dimethylphenyl)piperazine-1-carbodithioate

Guidance literature:: In toluene; byproducts: (CH3)2C6H3(C4H10N2)Cl; stoich. mixt. refluxed for 6-7 h with stirring; filtered off, evapd., recrystd. (MeOH/CHCl3), elem. anal.;
DOI:10.1016/j.poly.2011.10.025