1-carbamoylmethyl-1,2-dihydro-2-(4-toluenesulfonimido)-5-benzoylpyridine

Base Information

Chemical Name:1-carbamoylmethyl-1,2-dihydro-2-(4-toluenesulfonimido)-5-benzoylpyridine
CAS No.:220259-83-6
Molecular Formula:C₂₁H₁₉N₃O₄S
Molecular Weight:409.466
Hs Code.:

Synonyms:1-carbamoylmethyl-1,2-dihydro-2-(4-toluenesulfonimido)-5-benzoylpyridine

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Chemical Property of 1-carbamoylmethyl-1,2-dihydro-2-(4-toluenesulfonimido)-5-benzoylpyridine

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Technology Process of 1-carbamoylmethyl-1,2-dihydro-2-(4-toluenesulfonimido)-5-benzoylpyridine

There total 8 articles about 1-carbamoylmethyl-1,2-dihydro-2-(4-toluenesulfonimido)-5-benzoylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 144-48-9
iodacetamide

: 220259-66-5
1,2-dihydro-2-(p-toluenesulfonimido)-5-benzoylpyridine

: 220259-83-6
1-carbamoylmethyl-1,2-dihydro-2-(4-toluenesulfonimido)-5-benzoylpyridine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 24h;
DOI:10.1021/jm9810405

Reference yield: 97.0%

: 144-48-9
iodacetamide

: 220259-66-5
1,2-dihydro-2-toluenesulfonimido-5-benzoylpyridine

: 220259-83-6
1-carbamoylmethyl-1,2-dihydro-2-(4-toluenesulfonimido)-5-benzoylpyridine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 24h;
DOI:10.1016/S0040-4020(98)01052-7

Reference yield:

: 58757-38-3
6-Chloronicotinoyl chloride

: 220259-83-6
1-carbamoylmethyl-1,2-dihydro-2-(4-toluenesulfonimido)-5-benzoylpyridine

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / AlCl₃ / Heating

2: 85 percent / NH₃ / ethanol / 16 h / 145 °C

3: 91 percent / pyridine / 80 - 90 °C

4: 97 percent / DIPEA / dimethylformamide / 24 h

With pyridine; aluminium trichloride; ammonia; N-ethyl-N,N-diisopropylamine; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm9810405