(1S,2S)-1--1-(methoxycarbonyl)-2-(2-(methoxycarbonyl)ethyl)cyclopropane

Base Information

Chemical Name:(1S,2S)-1--1-(methoxycarbonyl)-2-(2-(methoxycarbonyl)ethyl)cyclopropane
CAS No.:161111-18-8
Molecular Formula:C₁₇H₂₁NO₆
Molecular Weight:335.357
Hs Code.:

(1S,2S)-1-<N-((Benzyloxy)carbonyl)amino>-1-(methoxycarbonyl)-2-(2-(methoxycarbonyl)ethyl)cyclopropane

Synonyms:(1S,2S)-1--1-(methoxycarbonyl)-2-(2-(methoxycarbonyl)ethyl)cyclopropane

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Chemical Property of (1S,2S)-1--1-(methoxycarbonyl)-2-(2-(methoxycarbonyl)ethyl)cyclopropane

Chemical Property:

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Technology Process of (1S,2S)-1--1-(methoxycarbonyl)-2-(2-(methoxycarbonyl)ethyl)cyclopropane

There total 5 articles about (1S,2S)-1--1-(methoxycarbonyl)-2-(2-(methoxycarbonyl)ethyl)cyclopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 67-56-1
methanol

: 161111-17-7
(1S,2S)-1--1-(methoxycarbonyl)-2-(2-cyanoethyl)cyclopropane

: 161111-18-8
(1S,2S)-1--1-(methoxycarbonyl)-2-(2-(methoxycarbonyl)ethyl)cyclopropane

Guidance literature:: With hydrogenchloride; In diethyl ether; for 1.5h; Ambient temperature;
DOI:10.1021/jo00097a040

Reference yield:

: 161111-14-4
(1S,6R)-1--3-oxabicyclo<4.1.0>-2-heptanone

: 161111-18-8
(1S,2S)-1--1-(methoxycarbonyl)-2-(2-(methoxycarbonyl)ethyl)cyclopropane

Guidance literature:: Multi-step reaction with 5 steps

1: aq. LiOH / tetrahydrofuran / Ambient temperature

2: K₂CO₃ / acetonitrile; dimethylformamide

3: 100 percent / TEA / CH₂Cl₂ / 0.5 h

4: 94 percent / NaI / dimethylformamide / 2 h / 80 °C

5: 94 percent / HCl / diethyl ether / 1.5 h / Ambient temperature

With hydrogenchloride; lithium hydroxide; TEA; potassium carbonate; sodium iodide; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo00097a040

Reference yield:

: 161111-15-5
Methyl (1S,2R)-1--2-(2-hydroxyethyl)cyclopropanecarboxylate

: 161111-18-8
(1S,2S)-1--1-(methoxycarbonyl)-2-(2-(methoxycarbonyl)ethyl)cyclopropane

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / TEA / CH₂Cl₂ / 0.5 h

2: 94 percent / NaI / dimethylformamide / 2 h / 80 °C

3: 94 percent / HCl / diethyl ether / 1.5 h / Ambient temperature

With hydrogenchloride; TEA; sodium iodide; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00097a040