Technology Process of C25H37IN2O5
There total 6 articles about C25H37IN2O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(1S,2S,3S,5R)-(+)-isopinocampheylamine;
With
trimethylaluminum;
In
hexanes; dichloromethane;
for 0.25h;
C15H18INO5;
In
hexanes; dichloromethane;
at 20 ℃;
With
rochelle salt;
In
hexanes; dichloromethane; water;
for 2h;
- Guidance literature:
-
(1S,2S,3S,5R)-(+)-isopinocampheylamine;
With
trimethylaluminum;
In
hexane; dichloromethane;
for 0.25h;
C15H18INO5;
In
hexane; dichloromethane;
at 20 ℃;
With
Rochelle's salt;
In
hexane; dichloromethane; water;
for 2h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 24 h / 0 - 20 °C
2.1: potassium hydroxide; hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 16 h / 20 °C / pH 9
3.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 16 h / pH 2
3.2: pH 7 / Alkaline aqueous solution
4.1: benzene / Heating / reflux
5.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation
5.2: 2 h
6.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 4 h / 20 °C
7.1: trimethylaluminum / hexane; dichloromethane / 0.25 h
7.2: 20 °C
7.3: 2 h
With
titanium(IV) isopropylate; hydrogenchloride; potassium hydroxide; hydroxylamine hydrochloride; methyl orange; trimethylaluminum; sodium hydride; sodium cyanoborohydride; pyridine hydrogenfluoride;
In
tetrahydrofuran; pyridine; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene; benzene;
