(2S,3S)-3-(t-Boc-amino)-4-cyclohexyl-1-(cyclohexylthio)-2-hydroxybutane

Base Information

Chemical Name:(2S,3S)-3-(t-Boc-amino)-4-cyclohexyl-1-(cyclohexylthio)-2-hydroxybutane
CAS No.:110206-05-8
Molecular Formula:C₂₁H₃₉NO₃S
Molecular Weight:385.612
Hs Code.:

Synonyms:(2S,3S)-3-(t-Boc-amino)-4-cyclohexyl-1-(cyclohexylthio)-2-hydroxybutane

Suppliers and Price of (2S,3S)-3-(t-Boc-amino)-4-cyclohexyl-1-(cyclohexylthio)-2-hydroxybutane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S)-3-(t-Boc-amino)-4-cyclohexyl-1-(cyclohexylthio)-2-hydroxybutane

Chemical Property:

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Technology Process of (2S,3S)-3-(t-Boc-amino)-4-cyclohexyl-1-(cyclohexylthio)-2-hydroxybutane

There total 1 articles about (2S,3S)-3-(t-Boc-amino)-4-cyclohexyl-1-(cyclohexylthio)-2-hydroxybutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1569-69-3
Cyclohexanethiol

: 107202-61-9
(2R,3S)-3-(t-butoxycarbonylamino)-4-cyclohexyl-1,2-epoxybutane

: 110206-05-8
(2S,3S)-3-(t-Boc-amino)-4-cyclohexyl-1-(cyclohexylthio)-2-hydroxybutane

: 110205-76-0
(2R,3S)-3-(t-Boc-amino)-4-cyclohexyl-1-(cyclohexylthio)-2-hydroxybutane

Guidance literature:: With triethylamine; In methanol; for 2h; Heating;
DOI:10.1021/jm00394a035

Reference yield:

: 110206-05-8
(2S,3S)-3-(t-Boc-amino)-4-cyclohexyl-1-(cyclohexylthio)-2-hydroxybutane

: (2S,3S)-3-Amino-4-cyclohexyl-1-cyclohexylsulfanyl-butan-2-ol

Guidance literature:: With hydrogenchloride; In ethanol; Ambient temperature;
DOI:10.1021/jm00394a035

Reference yield:

: 110206-05-8
(2S,3S)-3-(t-Boc-amino)-4-cyclohexyl-1-(cyclohexylthio)-2-hydroxybutane

: 103127-82-8
[(S)-1-((1S,2S)-1-Cyclohexylmethyl-3-cyclohexylsulfanyl-2-hydroxy-propylcarbamoyl)-2-(1H-imidazol-4-yl)-ethyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: HCl / ethanol / Ambient temperature

2: 1-hydroxybenzotriazole monohydrate (HOBt), N-methylmorpholine, 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide hydrochloride / dimethylformamide / -23 - 20 °C

With 4-methyl-morpholine; hydrogenchloride; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00394a035