(2R,3S)-3-(t-Boc-amino)-4-cyclohexyl-1-(cyclohexylthio)-2-hydroxybutane

Base Information

• Chemical Name: (2R,3S)-3-(t-Boc-amino)-4-cyclohexyl-1-(cyclohexylthio)-2-hydroxybutane
• CAS No.: 110205-76-0
• Molecular Formula: C₂₁H₃₉NO₃S
• Molecular Weight: 385.612

Synonyms:(2R,3S)-3-(t-Boc-amino)-4-cyclohexyl-1-(cyclohexylthio)-2-hydroxybutane

Chemical Property of (2R,3S)-3-(t-Boc-amino)-4-cyclohexyl-1-(cyclohexylthio)-2-hydroxybutane

Chemical Property:

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Technology Process of (2R,3S)-3-(t-Boc-amino)-4-cyclohexyl-1-(cyclohexylthio)-2-hydroxybutane

There total 1 articles about (2R,3S)-3-(t-Boc-amino)-4-cyclohexyl-1-(cyclohexylthio)-2-hydroxybutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

Cyclohexanethiol (1569-69-3) + (2R,3S)-3-(t-butoxycarbonylamino)-4-cyclohexyl-1,2-epoxybutane (107202-61-9) → (2S,3S)-3-(t-Boc-amino)-4-cyclohexyl-1-(cyclohexylthio)-2-hydroxybutane (110206-05-8) + (2R,3S)-3-(t-Boc-amino)-4-cyclohexyl-1-(cyclohexylthio)-2-hydroxybutane (110205-76-0)

Guidance literature:

With triethylamine; In methanol; for 2h; Heating;

DOI:10.1021/jm00394a035

Reference yield: 97.0%

(2R,3S)-3-(t-Boc-amino)-4-cyclohexyl-1-(cyclohexylthio)-2-hydroxybutane (110205-76-0) → (2R,3S)-3-(t-Boc-amino)-4-cyclohexyl-1-(cyclohexylsulfonyl)-2-hydroxybutane (110206-08-1)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 1h;

DOI:10.1021/jm00394a035

Reference yield:

(2R,3S)-3-(t-Boc-amino)-4-cyclohexyl-1-(cyclohexylthio)-2-hydroxybutane (110205-76-0) → (2R,3S)-3-Amino-4-cyclohexyl-1-cyclohexylsulfanyl-butan-2-ol; hydrochloride (103127-65-7)

Guidance literature:

With hydrogenchloride; In ethanol; Ambient temperature;

DOI:10.1021/jm00394a035

upstream raw materials:

Cyclohexanethiol

(2R,3S)-3-(t-butoxycarbonylamino)-4-cyclohexyl-1,2-epoxybutane

Downstream raw materials:

(2R,3S)-3-(t-Boc-amino)-4-cyclohexyl-1-(cyclohexylsulfonyl)-2-hydroxybutane

(2R,3S)-3-Amino-4-cyclohexyl-1-cyclohexylsulfanyl-butan-2-ol; hydrochloride

(2R,3S)-4-cyclohexyl-1-(cyclohexylsulfonyl)-2-hydroxybutane

(2R,3S)-3-<amino>-4-cyclohexyl-1-(cyclohexylsulfonyl)-2-hydroxybutane

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