2-(2,4-dinitrophenylsulfanyl)-1-(3-(4-methoxyphenyl)isoxazol-4-ylmethyl)-1H-benzoimidazole

Base Information

Chemical Name:2-(2,4-dinitrophenylsulfanyl)-1-(3-(4-methoxyphenyl)isoxazol-4-ylmethyl)-1H-benzoimidazole
CAS No.:1429494-47-2
Molecular Formula:C₂₄H₁₇N₅O₆S
Molecular Weight:503.495
Hs Code.:

Synonyms:2-(2,4-dinitrophenylsulfanyl)-1-(3-(4-methoxyphenyl)isoxazol-4-ylmethyl)-1H-benzoimidazole

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Chemical Property of 2-(2,4-dinitrophenylsulfanyl)-1-(3-(4-methoxyphenyl)isoxazol-4-ylmethyl)-1H-benzoimidazole

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Technology Process of 2-(2,4-dinitrophenylsulfanyl)-1-(3-(4-methoxyphenyl)isoxazol-4-ylmethyl)-1H-benzoimidazole

There total 4 articles about 2-(2,4-dinitrophenylsulfanyl)-1-(3-(4-methoxyphenyl)isoxazol-4-ylmethyl)-1H-benzoimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1424375-05-2
C₁₆H₁₀N₄O₄S

: 15500-73-9
4-methoxybenzonitrile oxide

: 1429494-47-2
2-(2,4-dinitrophenylsulfanyl)-1-(3-(4-methoxyphenyl)isoxazol-4-ylmethyl)-1H-benzoimidazole

: 1424375-24-5
C₂₄H₁₇N₅O₆S

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 16h; Overall yield = 68 %; Inert atmosphere;
DOI:10.1016/j.bmcl.2012.12.101

Reference yield:

: 95-54-5
1,2-diamino-benzene

: 1429494-47-2
2-(2,4-dinitrophenylsulfanyl)-1-(3-(4-methoxyphenyl)isoxazol-4-ylmethyl)-1H-benzoimidazole

: 1424375-24-5
C₂₄H₁₇N₅O₆S

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / water; ethanol / 100 °C

2: potassium hydroxide / water; ethanol / 3 h / Reflux

3: potassium carbonate / toluene; acetone / 5 h / Reflux

4: triethylamine / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

With potassium carbonate; triethylamine; potassium hydroxide; sodium hydroxide; In ethanol; dichloromethane; water; acetone; toluene;
DOI:10.1016/j.bmcl.2012.12.101

Reference yield:

: 583-39-1,2080-59-3
2,3-dihydrobenzimidazol-2-thione

: 1429494-47-2
2-(2,4-dinitrophenylsulfanyl)-1-(3-(4-methoxyphenyl)isoxazol-4-ylmethyl)-1H-benzoimidazole

: 1424375-24-5
C₂₄H₁₇N₅O₆S

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / water; ethanol / 3 h / Reflux

2: potassium carbonate / toluene; acetone / 5 h / Reflux

3: triethylamine / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

With potassium carbonate; triethylamine; potassium hydroxide; In ethanol; dichloromethane; water; acetone; toluene;
DOI:10.1016/j.bmcl.2012.12.101