Methyl (3S,6S)-1,2-bis(benzyloxycarbonyl)-1,2,3,6-tetrahydro-6-(2`,3`,4`,6`-tetra-O-acetyl-β-D-glucopyranosyloxy)pyridazine-3-carboxylate

Base Information Edit

Chemical Name:Methyl (3S,6S)-1,2-bis(benzyloxycarbonyl)-1,2,3,6-tetrahydro-6-(2`,3`,4`,6`-tetra-O-acetyl-β-D-glucopyranosyloxy)pyridazine-3-carboxylate
CAS No.:252039-93-3
Molecular Formula:C₃₆H₄₀N₂O₁₆
Molecular Weight:756.717
Hs Code.:
Mol file:252039-93-3.mol

Synonyms:Methyl (3S,6S)-1,2-bis(benzyloxycarbonyl)-1,2,3,6-tetrahydro-6-(2`,3`,4`,6`-tetra-O-acetyl-β-D-glucopyranosyloxy)pyridazine-3-carboxylate

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Chemical Property of Methyl (3S,6S)-1,2-bis(benzyloxycarbonyl)-1,2,3,6-tetrahydro-6-(2`,3`,4`,6`-tetra-O-acetyl-β-D-glucopyranosyloxy)pyridazine-3-carboxylate Edit

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Technology Process of Methyl (3S,6S)-1,2-bis(benzyloxycarbonyl)-1,2,3,6-tetrahydro-6-(2`,3`,4`,6`-tetra-O-acetyl-β-D-glucopyranosyloxy)pyridazine-3-carboxylate

There total 2 articles about Methyl (3S,6S)-1,2-bis(benzyloxycarbonyl)-1,2,3,6-tetrahydro-6-(2`,3`,4`,6`-tetra-O-acetyl-β-D-glucopyranosyloxy)pyridazine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 2449-05-0
dibenzyl azodicarboxylate

: 152094-22-9
Benzyl (2E,4E)-5-(2`,3`,4`,6`-tetra-O-acetyl-β-D-glucopyranoyloxy)penta-2,4-dienoate

: 252039-93-3
Methyl (3S,6S)-1,2-bis(benzyloxycarbonyl)-1,2,3,6-tetrahydro-6-(2`,3`,4`,6`-tetra-O-acetyl-β-D-glucopyranosyloxy)pyridazine-3-carboxylate

Guidance literature:: In toluene; at 90 ℃; for 18h;

Reference yield:

: 106758-59-2
(2E)-3-(2`,3`,4`,6`-tetra-O-acetyl-Β-D-glucopyranosyloxy)propenal

: 252039-93-3
Methyl (3S,6S)-1,2-bis(benzyloxycarbonyl)-1,2,3,6-tetrahydro-6-(2`,3`,4`,6`-tetra-O-acetyl-β-D-glucopyranosyloxy)pyridazine-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / CH₂Cl₂ / 18 h

2: 87 percent / toluene / 18 h / 90 °C

In dichloromethane; toluene; 1: Condensation / 2: Cycloaddition;