exo-10,10-diphenyl-10-methoxymethyl-7,7-dimethylbicyclo-[2.2.1]heptane-2-ol

Base Information

Chemical Name:exo-10,10-diphenyl-10-methoxymethyl-7,7-dimethylbicyclo-[2.2.1]heptane-2-ol
CAS No.:249739-60-4
Molecular Formula:C₂₃H₂₈O₂
Molecular Weight:336.474
Hs Code.:

Synonyms:exo-10,10-diphenyl-10-methoxymethyl-7,7-dimethylbicyclo-[2.2.1]heptane-2-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of exo-10,10-diphenyl-10-methoxymethyl-7,7-dimethylbicyclo-[2.2.1]heptane-2-ol

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Technology Process of exo-10,10-diphenyl-10-methoxymethyl-7,7-dimethylbicyclo-[2.2.1]heptane-2-ol

There total 5 articles about exo-10,10-diphenyl-10-methoxymethyl-7,7-dimethylbicyclo-[2.2.1]heptane-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 249739-53-5
exo-10,10-diphenyl-10-methoxymethyl-7,7-dimethylbicyclo[2.2.1]heptane-2-one

: 249739-60-4
exo-10,10-diphenyl-10-methoxymethyl-7,7-dimethylbicyclo-[2.2.1]heptane-2-ol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1021/jo9902188

Reference yield:

: 125637-45-8
(1S,4R)-7,7-dimethyl-2-oxobicyclo[2.2.1]heptane-1-carboxylic acid methylester

: 249739-60-4
exo-10,10-diphenyl-10-methoxymethyl-7,7-dimethylbicyclo-[2.2.1]heptane-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / tetrahydrofuran / 0.5 h / 0 °C

2: 77 percent / NaH / tetrahydrofuran / 0.5 h / 0 - 20 °C

3: 89 percent / LAH / tetrahydrofuran / -78 - 20 °C

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran; 1: Grignard reaction / 2: Methylation / 3: Reduction;
DOI:10.1021/jo9902188

Reference yield:

: 221099-70-3
exo-10,10-diphenyl-10-hydroxymethyl-7,7-dimethylbicyclo[2.2.1]heptane-2-one

: 249739-60-4
exo-10,10-diphenyl-10-methoxymethyl-7,7-dimethylbicyclo-[2.2.1]heptane-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / NaH / tetrahydrofuran / 0.5 h / 0 - 20 °C

2: 89 percent / LAH / tetrahydrofuran / -78 - 20 °C

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran; 1: Methylation / 2: Reduction;
DOI:10.1021/jo9902188