exo-10,10-diphenyl-10-methoxymethyl-7,7-dimethylbicyclo[2.2.1]heptane-2-one

Base Information

Chemical Name:exo-10,10-diphenyl-10-methoxymethyl-7,7-dimethylbicyclo[2.2.1]heptane-2-one
CAS No.:249739-53-5
Molecular Formula:C₂₃H₂₆O₂
Molecular Weight:334.458
Hs Code.:

Synonyms:exo-10,10-diphenyl-10-methoxymethyl-7,7-dimethylbicyclo[2.2.1]heptane-2-one

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Chemical Property of exo-10,10-diphenyl-10-methoxymethyl-7,7-dimethylbicyclo[2.2.1]heptane-2-one

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Technology Process of exo-10,10-diphenyl-10-methoxymethyl-7,7-dimethylbicyclo[2.2.1]heptane-2-one

There total 4 articles about exo-10,10-diphenyl-10-methoxymethyl-7,7-dimethylbicyclo[2.2.1]heptane-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 221099-70-3
exo-10,10-diphenyl-10-hydroxymethyl-7,7-dimethylbicyclo[2.2.1]heptane-2-one

: 74-88-4
methyl iodide

: 249739-53-5
exo-10,10-diphenyl-10-methoxymethyl-7,7-dimethylbicyclo[2.2.1]heptane-2-one

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 0.5h;
DOI:10.1021/jo9902188

Reference yield:

: 125637-45-8
(1S,4R)-7,7-dimethyl-2-oxobicyclo[2.2.1]heptane-1-carboxylic acid methylester

: 249739-53-5
exo-10,10-diphenyl-10-methoxymethyl-7,7-dimethylbicyclo[2.2.1]heptane-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / tetrahydrofuran / 0.5 h / 0 °C

2: 77 percent / NaH / tetrahydrofuran / 0.5 h / 0 - 20 °C

With sodium hydride; In tetrahydrofuran; 1: Grignard reaction / 2: Methylation;
DOI:10.1021/jo9902188

Reference yield:

: phenylmagnesium bromide

: 249739-53-5
exo-10,10-diphenyl-10-methoxymethyl-7,7-dimethylbicyclo[2.2.1]heptane-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / tetrahydrofuran / 0.5 h / 0 °C

2: 77 percent / NaH / tetrahydrofuran / 0.5 h / 0 - 20 °C

With sodium hydride; In tetrahydrofuran; 1: Grignard reaction / 2: Methylation;
DOI:10.1021/jo9902188