1-α-D-(5'-O-tert-butyldiphenyIsiIanoxyl-2',3'-di-O-trimethylacetyl-arabinofuranosyl)-2-nitroimidazole

Base Information

Chemical Name:1-α-D-(5'-O-tert-butyldiphenyIsiIanoxyl-2',3'-di-O-trimethylacetyl-arabinofuranosyl)-2-nitroimidazole
CAS No.:1352939-26-4
Molecular Formula:C₃₄H₄₅N₃O₈Si
Molecular Weight:651.832
Hs Code.:

Synonyms:1-α-D-(5'-O-tert-butyldiphenyIsiIanoxyl-2',3'-di-O-trimethylacetyl-arabinofuranosyl)-2-nitroimidazole

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Chemical Property of 1-α-D-(5'-O-tert-butyldiphenyIsiIanoxyl-2',3'-di-O-trimethylacetyl-arabinofuranosyl)-2-nitroimidazole

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Technology Process of 1-α-D-(5'-O-tert-butyldiphenyIsiIanoxyl-2',3'-di-O-trimethylacetyl-arabinofuranosyl)-2-nitroimidazole

There total 1 articles about 1-α-D-(5'-O-tert-butyldiphenyIsiIanoxyl-2',3'-di-O-trimethylacetyl-arabinofuranosyl)-2-nitroimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3282-30-2
pivaloyl chloride

: 83416-40-4
1-α-D-(arabinofuranosyl)-2-nitroimidazole

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1352939-26-4
1-α-D-(5'-O-tert-butyldiphenyIsiIanoxyl-2',3'-di-O-trimethylacetyl-arabinofuranosyl)-2-nitroimidazole

Guidance literature:: 1-α-D-(arabinofuranosyl)-2-nitroimidazole; tert-butylchlorodiphenylsilane; With pyridine; at 20 ℃; for 24h;

pivaloyl chloride; With pyridine; at 20 ℃; for 48h;

Reference yield:

: 1352939-26-4
1-α-D-(5'-O-tert-butyldiphenyIsiIanoxyl-2',3'-di-O-trimethylacetyl-arabinofuranosyl)-2-nitroimidazole

: 1352939-30-0
1-α-D-(5'-O-(4-nitrobenzenesulfonyI)-2',3'-di-O-pivaloyl-arabinofuranosyl)-2-nitroimidazole

Guidance literature:: Multi-step reaction with 2 steps

1: benzoic acid; potassium fluoride / acetonitrile / 12 h / 80 °C

2: dmap; pyridine / 16 h / 20 °C

With pyridine; dmap; potassium fluoride; benzoic acid; In acetonitrile;

Reference yield:

: 1352939-26-4
1-α-D-(5'-O-tert-butyldiphenyIsiIanoxyl-2',3'-di-O-trimethylacetyl-arabinofuranosyl)-2-nitroimidazole

: 1352939-32-2
1-α-D-(5'-O-(toluenesulfonyI)-2',3'-di-O-pivaloyl-arabinofuranosyl)-2-nitroimidazole

Guidance literature:: Multi-step reaction with 2 steps

1: benzoic acid; potassium fluoride / acetonitrile / 12 h / 80 °C

2: pyridine / 24 h / 0 - 22 °C

With pyridine; potassium fluoride; benzoic acid; In acetonitrile;