Trifluoro-methanesulfonic acid 3-[1-biphenyl-4-yl-meth-(E)-ylidene]-4-oxo-chroman-7-yl ester

Base Information

Chemical Name:Trifluoro-methanesulfonic acid 3-[1-biphenyl-4-yl-meth-(E)-ylidene]-4-oxo-chroman-7-yl ester
CAS No.:179107-86-9
Molecular Formula:C₂₃H₁₅F₃O₅S
Molecular Weight:460.43
Hs Code.:

Synonyms:Trifluoro-methanesulfonic acid 3-[1-biphenyl-4-yl-meth-(E)-ylidene]-4-oxo-chroman-7-yl ester

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Chemical Property of Trifluoro-methanesulfonic acid 3-[1-biphenyl-4-yl-meth-(E)-ylidene]-4-oxo-chroman-7-yl ester

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Technology Process of Trifluoro-methanesulfonic acid 3-[1-biphenyl-4-yl-meth-(E)-ylidene]-4-oxo-chroman-7-yl ester

There total 1 articles about Trifluoro-methanesulfonic acid 3-[1-biphenyl-4-yl-meth-(E)-ylidene]-4-oxo-chroman-7-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3218-36-8
4-Phenylbenzaldehyde

: 151884-08-1
4-oxochroman-7-yl trifluoromethanesulfonate

: 179107-86-9
Trifluoro-methanesulfonic acid 3-[1-biphenyl-4-yl-meth-(E)-ylidene]-4-oxo-chroman-7-yl ester

Guidance literature:: With pyrrolidine; In methanol; Ambient temperature;
DOI:10.1021/jm00046a001

Reference yield:

: 179107-86-9
Trifluoro-methanesulfonic acid 3-[1-biphenyl-4-yl-meth-(E)-ylidene]-4-oxo-chroman-7-yl ester

: 179107-69-8
Trifluoro-methanesulfonic acid 3-biphenyl-4-ylmethyl-4-oxo-chroman-7-yl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; under 2068.6 Torr; Yield given;
DOI:10.1021/jm00046a001

Reference yield:

: 179107-86-9
Trifluoro-methanesulfonic acid 3-[1-biphenyl-4-yl-meth-(E)-ylidene]-4-oxo-chroman-7-yl ester

: 179107-64-3
Ethyl 1-(3-(4-phenyl-phenylmethyl)-4-chromanon-7-yl)cyclopentane-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / ethyl acetate / 2068.6 Torr

2: 87 percent / Pd(PhCN)2Cl₂, ZnCl₂, P(o-tol)3 / dimethylformamide; 1,2-dimethoxy-ethane / 80 °C

With bis(benzonitrile)palladium(II) dichloride; hydrogen; tris-(o-tolyl)phosphine; zinc(II) chloride; palladium on activated charcoal; In 1,2-dimethoxyethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm00046a001