3,3',3,3',3,3'-(3,3',3-(4,4',4-(4,4',4-(4,4',4-(benzene-1,3,5-triyltris(methylene))tris(piperazine-4,1-diyl))tris(butane-4,1-diyl))tris(piperazine-4,1-diyl))tris(propane-3,1-diyl))tris(azanetriyl)hexapropanenitrile

Base Information

Chemical Name:3,3',3,3',3,3'-(3,3',3-(4,4',4-(4,4',4-(4,4',4-(benzene-1,3,5-triyltris(methylene))tris(piperazine-4,1-diyl))tris(butane-4,1-diyl))tris(piperazine-4,1-diyl))tris(propane-3,1-diyl))tris(azanetriyl)hexapropanenitrile
CAS No.:1278585-02-6
Molecular Formula:C₇₂H₁₂₃N₂₁
Molecular Weight:1282.91
Hs Code.:

3,3',3,3',3,3'-(3,3',3-(4,4',4-(4,4',4-(4,4',4-(benzene-1,3,5-triyltris(methylene))tris(piperazine-4,1-diyl))tris(butane-4,1-diyl))tris(piperazine-4,1-diyl))tris(propane-3,1-diyl))tris(azanetriyl)hexapropanenitrile

Synonyms:3,3',3,3',3,3'-(3,3',3-(4,4',4-(4,4',4-(4,4',4-(benzene-1,3,5-triyltris(methylene))tris(piperazine-4,1-diyl))tris(butane-4,1-diyl))tris(piperazine-4,1-diyl))tris(propane-3,1-diyl))tris(azanetriyl)hexapropanenitrile

Suppliers and Price of 3,3',3,3',3,3'-(3,3',3-(4,4',4-(4,4',4-(4,4',4-(benzene-1,3,5-triyltris(methylene))tris(piperazine-4,1-diyl))tris(butane-4,1-diyl))tris(piperazine-4,1-diyl))tris(propane-3,1-diyl))tris(azanetriyl)hexapropanenitrile

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Chemical Property of 3,3',3,3',3,3'-(3,3',3-(4,4',4-(4,4',4-(4,4',4-(benzene-1,3,5-triyltris(methylene))tris(piperazine-4,1-diyl))tris(butane-4,1-diyl))tris(piperazine-4,1-diyl))tris(propane-3,1-diyl))tris(azanetriyl)hexapropanenitrile

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Technology Process of 3,3',3,3',3,3'-(3,3',3-(4,4',4-(4,4',4-(4,4',4-(benzene-1,3,5-triyltris(methylene))tris(piperazine-4,1-diyl))tris(butane-4,1-diyl))tris(piperazine-4,1-diyl))tris(propane-3,1-diyl))tris(azanetriyl)hexapropanenitrile

There total 4 articles about 3,3',3,3',3,3'-(3,3',3-(4,4',4-(4,4',4-(4,4',4-(benzene-1,3,5-triyltris(methylene))tris(piperazine-4,1-diyl))tris(butane-4,1-diyl))tris(piperazine-4,1-diyl))tris(propane-3,1-diyl))tris(azanetriyl)hexapropanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 201230-82-2
carbon monoxide

: 1278584-89-6
3-[(2-cyano-ethyl)-(3-piperazin-1-yl-propyl)-amino]-propionitrile

: 1278585-01-5
1,3,5-tris((4-allylpiperazin-1-yl)methyl)benzene

: 1278585-02-6
3,3',3,3',3,3'-(3,3',3-(4,4',4-(4,4',4-(4,4',4-(benzene-1,3,5-triyltris(methylene))tris(piperazine-4,1-diyl))tris(butane-4,1-diyl))tris(piperazine-4,1-diyl))tris(propane-3,1-diyl))tris(azanetriyl)hexapropanenitrile

Guidance literature:: With acetylacetonatodicarbonylrhodium(l); hydrogen; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; methanol; at 80 ℃; for 120h; under 37503.8 Torr;
DOI:10.1002/ejoc.201001307

Reference yield:

: 944408-70-2
1-(3,5-bis((piperazin-1-yl)methyl)benzyl)piperazine

: 1278585-02-6
3,3',3,3',3,3'-(3,3',3-(4,4',4-(4,4',4-(4,4',4-(benzene-1,3,5-triyltris(methylene))tris(piperazine-4,1-diyl))tris(butane-4,1-diyl))tris(piperazine-4,1-diyl))tris(propane-3,1-diyl))tris(azanetriyl)hexapropanenitrile

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / 12 h / Reflux

2: acetylacetonatodicarbonylrhodium(l); hydrogen; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene / 1,4-dioxane; methanol / 120 h / 80 °C / 37503.8 Torr

With acetylacetonatodicarbonylrhodium(l); hydrogen; triethylamine; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; In 1,4-dioxane; methanol;
DOI:10.1002/ejoc.201001307

Reference yield:

: 373608-48-1
4-(3-aminopropyl)piperazine-1-carboxylic acid tert-butyl ester

: 1278585-02-6
3,3',3,3',3,3'-(3,3',3-(4,4',4-(4,4',4-(4,4',4-(benzene-1,3,5-triyltris(methylene))tris(piperazine-4,1-diyl))tris(butane-4,1-diyl))tris(piperazine-4,1-diyl))tris(propane-3,1-diyl))tris(azanetriyl)hexapropanenitrile

Guidance literature:: Multi-step reaction with 3 steps

1: water / Reflux

2: hydrogenchloride / 1,4-dioxane / 20 °C

3: acetylacetonatodicarbonylrhodium(l); hydrogen; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane; methanol / 120 h / 80 °C / 37503.8 Torr

With hydrogenchloride; acetylacetonatodicarbonylrhodium(l); hydrogen; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; methanol; water; 1: Michael addition;
DOI:10.1002/ejoc.201001307