Diethyl-thiocarbamic acid O-((2R,3S)-3-benzyloxy-5-methoxy-tetrahydro-furan-2-ylmethyl) ester

Base Information

Chemical Name:Diethyl-thiocarbamic acid O-((2R,3S)-3-benzyloxy-5-methoxy-tetrahydro-furan-2-ylmethyl) ester
CAS No.:189291-00-7
Molecular Formula:C₁₈H₂₇NO₄S
Molecular Weight:353.483
Hs Code.:

Synonyms:Diethyl-thiocarbamic acid O-((2R,3S)-3-benzyloxy-5-methoxy-tetrahydro-furan-2-ylmethyl) ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Diethyl-thiocarbamic acid O-((2R,3S)-3-benzyloxy-5-methoxy-tetrahydro-furan-2-ylmethyl) ester

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Technology Process of Diethyl-thiocarbamic acid O-((2R,3S)-3-benzyloxy-5-methoxy-tetrahydro-furan-2-ylmethyl) ester

There total 3 articles about Diethyl-thiocarbamic acid O-((2R,3S)-3-benzyloxy-5-methoxy-tetrahydro-furan-2-ylmethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 34212-65-2
Methyl 2-Deoxy-3-benzyl-D-ribofuranoside

: 88-11-9
N,N-diethylthiocarbamoyl chloride

: 189291-00-7
Diethyl-thiocarbamic acid O-((2R,3S)-3-benzyloxy-5-methoxy-tetrahydro-furan-2-ylmethyl) ester

Guidance literature:: With sodium hydride; In tetrahydrofuran;
DOI:10.1246/cl.1997.389

Reference yield:

: 105386-65-0
methyl 5-O-(tert-butyldimethylsilyl)-2-deoxy-α,β-D-erythropentofuranoside

: 189291-00-7
Diethyl-thiocarbamic acid O-((2R,3S)-3-benzyloxy-5-methoxy-tetrahydro-furan-2-ylmethyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: NaH, n-Bu₄NI / tetrahydrofuran

2: 95 percent / TBAF / tetrahydrofuran

3: 91 percent / NaH / tetrahydrofuran

With tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran;
DOI:10.1246/cl.1997.389

Reference yield:

: 105386-66-1
methyl 3-O-benzyl-5-O-(t-butyldimethylsilyl)-2-deoxyribofuranoside

: 189291-00-7
Diethyl-thiocarbamic acid O-((2R,3S)-3-benzyloxy-5-methoxy-tetrahydro-furan-2-ylmethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / TBAF / tetrahydrofuran

2: 91 percent / NaH / tetrahydrofuran

With tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran;
DOI:10.1246/cl.1997.389