5-(dimethylamino)-2-formylphenyl acetate

Base Information

Chemical Name:5-(dimethylamino)-2-formylphenyl acetate
CAS No.:174269-30-8
Molecular Formula:C₁₁H₁₃NO₃
Molecular Weight:207.229
Hs Code.:

Synonyms:5-(dimethylamino)-2-formylphenyl acetate

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Chemical Property of 5-(dimethylamino)-2-formylphenyl acetate

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Technology Process of 5-(dimethylamino)-2-formylphenyl acetate

There total 3 articles about 5-(dimethylamino)-2-formylphenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 41602-56-6
4-dimethylamino-2-hydroxy-benzaldehyde

: 75-36-5
acetyl chloride

: 174269-30-8
5-(dimethylamino)-2-formylphenyl acetate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;

Reference yield: 71.0%

: 41602-56-6
4-dimethylamino-2-hydroxy-benzaldehyde

: 108-24-7
acetic anhydride

: 174269-30-8
5-(dimethylamino)-2-formylphenyl acetate

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/jm2005404

Reference yield:

: 99-07-0
3-Dimethylaminophenol

: 174269-30-8
5-(dimethylamino)-2-formylphenyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: trichlorophosphate / 0.5 h / 0 °C

1.2: 4.5 h / 0 - 90 °C

2.1: triethylamine / dichloromethane / 0 - 20 °C

With triethylamine; trichlorophosphate; In dichloromethane;