2-chloro-6-phenyl-N-phenylcarbazole

Base Information

Chemical Name:2-chloro-6-phenyl-N-phenylcarbazole
CAS No.:1259388-66-3
Molecular Formula:C₂₄H₁₆ClN
Molecular Weight:353.851
Hs Code.:

Synonyms:2-chloro-6-phenyl-N-phenylcarbazole

Suppliers and Price of 2-chloro-6-phenyl-N-phenylcarbazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-chloro-6-phenyl-N-phenylcarbazole

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2-chloro-6-phenyl-N-phenylcarbazole

There total 6 articles about 2-chloro-6-phenyl-N-phenylcarbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1259388-64-1
2-chloro-6-bromo-N-phenylylcarbazole

: 98-80-6
phenylboronic acid

: 1259388-66-3
2-chloro-6-phenyl-N-phenylcarbazole

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; water; for 5h; Inert atmosphere; Reflux;

Reference yield:

: 577-19-5
2-nitrophenyl bromide

: 1259388-66-3
2-chloro-6-phenyl-N-phenylcarbazole

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; tetrahydrofuran / 8 h / Inert atmosphere; Reflux

2: triethyl phosphite / nitrogen / 24 h / 150 °C / Inert atmosphere

3: potassium carbonate / palladium diacetate; tri-tert-butyl phosphine / o-xylene / 24 h / 130 °C / Inert atmosphere

4: N-Bromosuccinimide / dichloromethane / 2 h / 20 °C / Inert atmosphere

5: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; tetrahydrofuran / 5 h / Inert atmosphere; Reflux

With N-Bromosuccinimide; sodium carbonate; potassium carbonate; triethyl phosphite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium diacetate; In tetrahydrofuran; dichloromethane; o-xylene; nitrogen; water;

Reference yield:

: 6271-80-3
4'-chloro-2-nitrobiphenyl

: 1259388-66-3
2-chloro-6-phenyl-N-phenylcarbazole

Guidance literature:: Multi-step reaction with 4 steps

1: triethyl phosphite / nitrogen / 24 h / 150 °C / Inert atmosphere

2: potassium carbonate / palladium diacetate; tri-tert-butyl phosphine / o-xylene / 24 h / 130 °C / Inert atmosphere

3: N-Bromosuccinimide / dichloromethane / 2 h / 20 °C / Inert atmosphere

4: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; tetrahydrofuran / 5 h / Inert atmosphere; Reflux

With N-Bromosuccinimide; sodium carbonate; potassium carbonate; triethyl phosphite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium diacetate; In tetrahydrofuran; dichloromethane; o-xylene; nitrogen; water;