4,6-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-N-(2-tritylsulfanyl-ethyl)-isophthalamic acid

Base Information

Chemical Name:4,6-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-N-(2-tritylsulfanyl-ethyl)-isophthalamic acid
CAS No.:936354-38-0
Molecular Formula:C₄₃H₅₃NO₁₁S
Molecular Weight:791.96
Hs Code.:

Synonyms:4,6-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-N-(2-tritylsulfanyl-ethyl)-isophthalamic acid

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Chemical Property of 4,6-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-N-(2-tritylsulfanyl-ethyl)-isophthalamic acid

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Technology Process of 4,6-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-N-(2-tritylsulfanyl-ethyl)-isophthalamic acid

There total 7 articles about 4,6-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-N-(2-tritylsulfanyl-ethyl)-isophthalamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₄H₅₅NO₁₁S

: 936354-38-0
4,6-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-N-(2-tritylsulfanyl-ethyl)-isophthalamic acid

Guidance literature:: With sodium hydroxide; In methanol;
DOI:10.1021/ja064515n

Reference yield:

: 874210-29-4
4,6-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}isophthalic acid dimethyl ester

: 936354-38-0
4,6-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-N-(2-tritylsulfanyl-ethyl)-isophthalamic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 3.5 g / NaOH / methanol; H₂O / 20 °C

2: 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide; N-hydroxybenzotriazole / CH₂Cl₂ / 20 h / 0 - 20 °C

3: NaOH / methanol

With sodium hydroxide; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In methanol; dichloromethane; water;
DOI:10.1021/ja064515n

Reference yield:

: 874210-38-5
4,6-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-isophthalic acid monomethyl ester

: 936354-38-0
4,6-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-N-(2-tritylsulfanyl-ethyl)-isophthalamic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide; N-hydroxybenzotriazole / CH₂Cl₂ / 20 h / 0 - 20 °C

2: NaOH / methanol

With sodium hydroxide; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In methanol; dichloromethane;
DOI:10.1021/ja064515n