2-(((tributylstannyl)methyl)thio)-N-(4-(trifluoromethyl)benzylidene)ethanamine

Base Information

Chemical Name:2-(((tributylstannyl)methyl)thio)-N-(4-(trifluoromethyl)benzylidene)ethanamine
CAS No.:1452829-10-5
Molecular Formula:C₂₃H₃₈F₃NSSn
Molecular Weight:536.333
Hs Code.:

Synonyms:2-(((tributylstannyl)methyl)thio)-N-(4-(trifluoromethyl)benzylidene)ethanamine

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Chemical Property of 2-(((tributylstannyl)methyl)thio)-N-(4-(trifluoromethyl)benzylidene)ethanamine

Chemical Property:

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Technology Process of 2-(((tributylstannyl)methyl)thio)-N-(4-(trifluoromethyl)benzylidene)ethanamine

There total 4 articles about 2-(((tributylstannyl)methyl)thio)-N-(4-(trifluoromethyl)benzylidene)ethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 688-73-3
tri-n-butyl-tin hydride

: 1452829-10-5
2-(((tributylstannyl)methyl)thio)-N-(4-(trifluoromethyl)benzylidene)ethanamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: diisopropylamine; n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 - 0 °C / Inert atmosphere

1.2: 4 h / 0 - 20 °C / Inert atmosphere

2.1: N-iodo-succinimide; triphenylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere

3.1: potassium carbonate / ethanol; water / 12 h / 70 °C / Inert atmosphere

4.1: dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve

With N-iodo-succinimide; n-butyllithium; potassium carbonate; diisopropylamine; triphenylphosphine; In tetrahydrofuran; ethanol; hexane; dichloromethane; water;
DOI:10.1002/anie.201208064

Reference yield:

: 27490-33-1
tri-n-butylstannylmethanol

: 1452829-10-5
2-(((tributylstannyl)methyl)thio)-N-(4-(trifluoromethyl)benzylidene)ethanamine

Guidance literature:: Multi-step reaction with 3 steps

1: N-iodo-succinimide; triphenylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere

2: potassium carbonate / ethanol; water / 12 h / 70 °C / Inert atmosphere

3: dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve

With N-iodo-succinimide; potassium carbonate; triphenylphosphine; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1002/anie.201208064

Reference yield:

: 66222-29-5
tri-n-butylstannylmethyl iodide

: 1452829-10-5
2-(((tributylstannyl)methyl)thio)-N-(4-(trifluoromethyl)benzylidene)ethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / ethanol; water / 12 h / 70 °C / Inert atmosphere

2: dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve

With potassium carbonate; In ethanol; dichloromethane; water;
DOI:10.1002/anie.201208064