Technology Process of Ethyl onate
There total 11 articles about Ethyl onate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 3 steps
1: pyridine / 16 h / Ambient temperature
2: 87 percent / N-iodosuccinimide (NIS), trifluoromethanesulfonic acid (TfOH) / 1,2-dichloro-ethane; diethyl ether / 0.08 h / 0 °C
3: 96 percent / aq. HOAc / 2 h / 50 °C
With
pyridine; N-iodo-succinimide; trifluorormethanesulfonic acid; acetic acid;
In
diethyl ether; 1,2-dichloro-ethane;
DOI:10.1016/S0040-4020(01)88191-6
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) KOtBu / 1.) MeOH, 2.) ethyl acetate, 15 min, room temperature
2: pyridine / 16 h / Ambient temperature
3: 87 percent / N-iodosuccinimide (NIS), trifluoromethanesulfonic acid (TfOH) / 1,2-dichloro-ethane; diethyl ether / 0.08 h / 0 °C
4: 96 percent / aq. HOAc / 2 h / 50 °C
With
pyridine; N-iodo-succinimide; trifluorormethanesulfonic acid; potassium tert-butylate; acetic acid;
In
diethyl ether; 1,2-dichloro-ethane;
DOI:10.1016/S0040-4020(01)88191-6