3-(1-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-6-(methylthio)-1H-pyrazolo[3,4-d]pyrimidin-4-ylamino)phenol

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Chemical Name:3-(1-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-6-(methylthio)-1H-pyrazolo[3,4-d]pyrimidin-4-ylamino)phenol
CAS No.:1583285-03-3
Molecular Formula:C₂₂H₂₀N₈OS
Molecular Weight:444.52
Hs Code.:

Synonyms:3-(1-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-6-(methylthio)-1H-pyrazolo[3,4-d]pyrimidin-4-ylamino)phenol

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Chemical Property of 3-(1-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-6-(methylthio)-1H-pyrazolo[3,4-d]pyrimidin-4-ylamino)phenol

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Technology Process of 3-(1-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-6-(methylthio)-1H-pyrazolo[3,4-d]pyrimidin-4-ylamino)phenol

There total 6 articles about 3-(1-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-6-(methylthio)-1H-pyrazolo[3,4-d]pyrimidin-4-ylamino)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1583284-79-0
1-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-4-chloro-6-(methylthio)-1H-pyrazolo[3,4-d]pyrimidine

: 591-27-5
m-Hydroxyaniline

: 1583285-03-3
3-(1-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-6-(methylthio)-1H-pyrazolo[3,4-d]pyrimidin-4-ylamino)phenol

Guidance literature:: In ethanol; for 12h; Reflux; Inert atmosphere;
DOI:10.1021/co500004e

Reference yield: 45.0%

: 1583284-89-2
3-(6-(methylthio)-1-(prop-2-ynyl)-1H-pyrazolo[3,4-d]pyrimidin-4-ylamino)phenol

: 100-44-7
benzyl chloride

: 1583285-03-3
3-(1-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-6-(methylthio)-1H-pyrazolo[3,4-d]pyrimidin-4-ylamino)phenol

Guidance literature:: With sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 125 ℃; for 0.166667h; Microwave irradiation;
DOI:10.1021/co500004e

Reference yield:

: 1583284-78-9
4-chloro-6-(methylthio)-1-(prop-2-ynyl)-1H-pyrazolo[3,4-d]pyrimidine

: 1583285-03-3
3-(1-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-6-(methylthio)-1H-pyrazolo[3,4-d]pyrimidin-4-ylamino)phenol

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 12 h / Reflux; Inert atmosphere

2: sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate / tert-butyl alcohol; water / 0.17 h / 125 °C / Microwave irradiation

With sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In ethanol; water; tert-butyl alcohol;
DOI:10.1021/co500004e