1,1-dimethylethyl 4-(2-{4-[(3-chloropropyl)oxy]phenyl}ethyl)-1-piperazinecarboxylate

Base Information

Chemical Name:1,1-dimethylethyl 4-(2-{4-[(3-chloropropyl)oxy]phenyl}ethyl)-1-piperazinecarboxylate
CAS No.:958651-16-6
Molecular Formula:C₂₀H₃₁ClN₂O₃
Molecular Weight:382.931
Hs Code.:

Synonyms:1,1-dimethylethyl 4-(2-{4-[(3-chloropropyl)oxy]phenyl}ethyl)-1-piperazinecarboxylate

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Chemical Property of 1,1-dimethylethyl 4-(2-{4-[(3-chloropropyl)oxy]phenyl}ethyl)-1-piperazinecarboxylate

Chemical Property:

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Technology Process of 1,1-dimethylethyl 4-(2-{4-[(3-chloropropyl)oxy]phenyl}ethyl)-1-piperazinecarboxylate

There total 5 articles about 1,1-dimethylethyl 4-(2-{4-[(3-chloropropyl)oxy]phenyl}ethyl)-1-piperazinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-70-6
1.3-chlorobromopropane

: 958651-16-6
1,1-dimethylethyl 4-(2-{4-[(3-chloropropyl)oxy]phenyl}ethyl)-1-piperazinecarboxylate

Guidance literature:: tert-butyl 4-[2-(4-hydroxyphenyl)ethyl]piperazine-1-carboxylate; With potassium carbonate; In butanone; at 20 ℃; for 1h;

1.3-chlorobromopropane; In butanone; at 20 ℃; Heating / reflux;

Reference yield:

: 620600-60-4
methanesulfonic acid 2-[4-(tert-butyl-dimethyl-silyloxy)-phenyl]-ethyl ester

: 958651-16-6
1,1-dimethylethyl 4-(2-{4-[(3-chloropropyl)oxy]phenyl}ethyl)-1-piperazinecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / acetonitrile / 48 h / Reflux

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

3: potassium carbonate / butanone / 24 h / Reflux

With tetrabutyl ammonium fluoride; sodium hydrogencarbonate; potassium carbonate; In tetrahydrofuran; acetonitrile; butanone;
DOI:10.1016/j.bmcl.2016.11.022

Reference yield:

: 958651-13-3
1,1-dimethylethyl 4-[2-(4-{[(1,1-dimethylethyl)(dimethyl)silyl]oxy}phenyl)ethyl]-1-piperazinecarboxylate

: 958651-16-6
1,1-dimethylethyl 4-(2-{4-[(3-chloropropyl)oxy]phenyl}ethyl)-1-piperazinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

2: potassium carbonate / butanone / 24 h / Reflux

With tetrabutyl ammonium fluoride; potassium carbonate; In tetrahydrofuran; butanone;
DOI:10.1016/j.bmcl.2016.11.022