1,1-dimethylethyl 4-[2-(4-{[3-(hexahydro-1H-azepin-1-yl)propyl]oxy}phenyl)ethyl]-1-piperazinecarboxylate

Base Information

Chemical Name:1,1-dimethylethyl 4-[2-(4-{[3-(hexahydro-1H-azepin-1-yl)propyl]oxy}phenyl)ethyl]-1-piperazinecarboxylate
CAS No.:958651-17-7
Molecular Formula:C₂₆H₄₃N₃O₃
Molecular Weight:445.646
Hs Code.:

Synonyms:1,1-dimethylethyl 4-[2-(4-{[3-(hexahydro-1H-azepin-1-yl)propyl]oxy}phenyl)ethyl]-1-piperazinecarboxylate

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Chemical Property of 1,1-dimethylethyl 4-[2-(4-{[3-(hexahydro-1H-azepin-1-yl)propyl]oxy}phenyl)ethyl]-1-piperazinecarboxylate

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Technology Process of 1,1-dimethylethyl 4-[2-(4-{[3-(hexahydro-1H-azepin-1-yl)propyl]oxy}phenyl)ethyl]-1-piperazinecarboxylate

There total 1 articles about 1,1-dimethylethyl 4-[2-(4-{[3-(hexahydro-1H-azepin-1-yl)propyl]oxy}phenyl)ethyl]-1-piperazinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 505-66-8
1,4-Diazacycloheptane

: 958651-16-6
1,1-dimethylethyl 4-(2-{4-[(3-chloropropyl)oxy]phenyl}ethyl)-1-piperazinecarboxylate

: 958651-17-7
1,1-dimethylethyl 4-[2-(4-{[3-(hexahydro-1H-azepin-1-yl)propyl]oxy}phenyl)ethyl]-1-piperazinecarboxylate

Guidance literature:: With potassium carbonate; potassium iodide; In butanone; for 16h; Heating / reflux;

Reference yield:

: 958651-17-7
1,1-dimethylethyl 4-[2-(4-{[3-(hexahydro-1H-azepin-1-yl)propyl]oxy}phenyl)ethyl]-1-piperazinecarboxylate

: 958651-19-9
1-[3-({4-[2-(1-piperazinyl)ethyl]phenyl}oxy)propyl]hexahydro-1H-azepine

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 5h;

Reference yield:

: 958651-17-7
1,1-dimethylethyl 4-[2-(4-{[3-(hexahydro-1H-azepin-1-yl)propyl]oxy}phenyl)ethyl]-1-piperazinecarboxylate

: 958651-29-1
ethyl 3-(8-{4-[2-(4-{[3-(hexahydro-1H-azepin-1-yl)propyl]oxy}phenyl)ethyl]-1-piperazinyl}-2-quinolinyl)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid / dichloromethane / 5 h

2: caesium carbonate / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; DavePhos / tetrahydrofuran / Heating / reflux

3: hydrogen / palladium 10% on activated carbon / ethyl acetate

With hydrogen; caesium carbonate; trifluoroacetic acid; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium 10% on activated carbon; DavePhos; In tetrahydrofuran; dichloromethane; ethyl acetate;